GCMS calibration data, June 10 2002

2 z Quantitation Report (QT Reviewed) - K o o CO g Data File C:\MSDCHEM\l\DATA\060602\603REFl .D Vial: 4 — o Acq On 6 Jun 2002 1:45 pm Operator: McLean "0 1 o Sample 6/3 eh Inst : Instrumen C O o Mise o o Multiplr: 1.00 o' MS Integration Params: EVENTS.E "0 CH o CD Quant Time: Jun 10 10:18 2002 Quant Results File: 060302.RES — 0 o o Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Q C Title : 508 Modified GC/MS scan 3 Last Update : Thu Jun 06 15:03:45 2002 CD X Response via : Initial Calibration Abundance TlC:603REF1.D 2600000 o 2400000 8 o i 1 g E 2200000 f 0 £to § £ 2000000' 8 1800000 a 8 | 1600000 || 1400000 &

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1 1 1 1 1 1 f ' TT t"u f "IIT 11* 1 '1 ' I K . t N inl AA Time—> 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 ' ' 34'00 ' ' 36.00 ' ' 38.00 603REF1.D 060302.M Mon Jun 10 10:18:58 2002 Page 3