GCMS analysis results for unknown compounds, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\060702\12739.D Vial: 15 Acq On 7 Jun 2002 7:58 pm Operator: Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 7 Pyridine-d5- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 4.06 1.78 ug/L 1415000 1,4-dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pyridine-d5- 84 C5D5N 007291-22-7 9 2 Krypton 84 Kr 007439-90-9 b 3 Methanethiol 48 CH4S 000074-93-1/7 4 Methanethiol 48 CH4S 000074-93-1 7 Abundance Scan 167 (4.061 min): 12739.D (-166) (-) m/z 84.00 100/00% 47 84 88 50 5000 41 44 3.80 4.00 4.20 4.40 36 Ot " i" " i" ■' i" " I" “ i • ■' ■ i ■ ■ “ i' “ ■ i -m-p- mpmp T ‘1’171117 m/z 47.00 92.46% miz-> Abundance 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 «) 95 #33686: Pyridine-d5- 56 84 P 5000 52 28 3.80 4.00 4.20 4.40 m/z 88.00 72.63% 38 42 /"*

n/z-> 14 32.44+ 4241 ol ■ ■ I' ■'11" " I" " I" ■' 111 1 — 48 Illi

5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 62 66 76 11" "111" 111

Abundance #33829: Krypton MW 84

3.80 4.00 4.20 4.40 5000 m/z /* 48.10 61.85%

42 80 O+ —Imommmphpt TIPPTLPLPTTTT • ■ -1• • । * l1 ■ m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #111010: Methanethiol 47 3.80 4.00 4.20 4.40 m/ 50.05 61.42% 5000

15 0 .121.117724., -33 44 50 MImmmmRPTTTTIT n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.80 4.00 4.20 4.40

12739.D 060302.M Mon Jun 10 11:51:05 2002 Page 10

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