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← Document results/DEP Box 15/GCMS X 5/31/02 A 6/3/02
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GCMS analysis results for sample AE12279, June 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE12224 with surrogate recovery data and identification of unknown compounds.

NYC-WTC_000015075–000015083

Folder label: “GCMS X 5/31/02 A 6/3/02

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Scanned page image, NYC-WTC_000015080
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NYC 9/11 Public Portal Document LSC Area Percent Report

: Data File : C:\HPCHEM\1\DATA\JUN0302\12279.D Vial: 7 Acq On : 3 Jun 2002 3:05 pm Operator: Sample : re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline -drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.081 327 331 343 rBV2 41241 81656 2.00% 0.367% 2 12.065 760 765 790 rBV 1231533 2953001 72.17% 13.286% 3 15.691 1154 1160 1177 rBV 1838570 4015682 98.14% 18.067% 4 20.997 1731 1738 1750 rBV 1828427 4027022 98.42% 18.118% 5 23.136 1962 1971 1978 rBV 974634 2046126 50.00% 9.206% 6 25.431 2213 2221 2231 rBV 1873043 4091855 100.00% 18.410% 7 33.473 3090 3097 3117 rBV2 1246105 2926150 71.51% 13.165% 8 37.659 3545 3553 3568 rBV2 721938 2085043 50.96% 9.381%

Sum of corrected areas: 22226535 12279.D GCMS0531.M Tue Jun 04 09:03:31 2002

NYC-WTC_000015080

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NYC-WTC_000015080Source: NYC Law Department, mirrored locally

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