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GCMS analysis results for sample AE12279, June 2002

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Laboratory report documenting GCMS analysis of sample AE12224 with surrogate recovery data and identification of unknown compounds.

NYC-WTC_000015075–000015083

Folder label: “GCMS X 5/31/02 A 6/3/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C: \ HPCHEM\ 1 \DATA\ JUNO 302\12279.D Vial: 7 Acq On 3 Jun 2002 3:05 pm Operator : Sample re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jun 3 15:55 2002 Quant Results File :GCMS0531. RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 09:43:55 2002 Response via : Initial Calibration DataAcq Meth : GCMS0531

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.06 152 540638 40.00 ug/1 -0.01 10) Naphthalene-d8 15.69 136 2180598 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.00 164 1021483 40.00 ug/1 0.00 30) Phenanthrene-diO 25.43 188 1582629 40.00 ug/1 0.00 38) Chrysene-dl2 33.47 240 929411 40.00 ug/1 -0.03 44) Perylene-dl2 37.66 264 565235 40.00 ug/1 -0.02 System Monitoring Compounds 28) TCMX 23.14 209 220179 31.16 ug/L -0.01 Spiked Amount 40.000 Recovery 77.90% Target Compounds Qvalue 2) N-nitrosodimethylamine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 12.06 146 451 N.D. 5) 1,4-Dichlorobenzene 12.06 146 451 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2’-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.76 128 509 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.48 149 871 N.D. 26) 4-Chlorophenylphenylether 23.14 204 1302 N.D. 27) Fluorene 0.00 166 0 N.D. 2 9) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.14 168 495 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 3 3) Hexachiorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.49 178 224 N.D. (#) = qualifier out of range (m) = manual integration 12279.D GCMS0531.M Mon Jun 03 15:55:33 2002 Page 1

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