GCMS analysis results for sample AE12573, June 2002

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Laboratory report documenting GCMS analysis of sample AE12573 conducted on June 7, 2002, including surrogate recovery data.

NYC-WTC_000014710–000014719

Folder label: “GCMS X 5/28/02 A 6/4/02”

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\JUNO 302\12573.D Vial: 24 Acq On 4 Jun 2002 7:55 am Operator: Sample gc/ms scan 5/28 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jun 4 11:49 2002 Quant Results File: GCMS0531.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 09:43:55 2002 Response via : Initial Calibration DataAcq Meth : GCMS0531

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.06 152 495292 40.00 ug/1 -0.01 10) Naphthalene-d8 15.69 136 1977033 40.00 ug/1 -0.02 17) Acenaphthene-diO 20.99 164 959283 40.00 ug/1 -0.01 30) Phenanthrene-dlO 25.42 188 1439912 40.00 ug/1 -0.01 38) Chrysene-dl2 33.47 240 816046 40.00 ug/1 -0.03 44) Perylene-dl2 37.65 264 467336 40.00 ug/1 -0.03

System Monitoring Compounds 28) TCMX 23.14 209 186559 :28.11 ug/L -0.01 Spiked Amount 40.000 Recovery 70.28% Target Compounds Qvalue 2) N-nitrosodimethylamine 5.42 74 512 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-bichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 . N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.75 128 421 N.D. 16) Hexachiorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Ac enapht hene 0.00 153 0 N.D. . 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.48 149 310 N.D. 26) 4-Chlorophenylphenylether 23.13 204 995 -N.D. 27) Fluorene 0.00 166 0 N.D. 2 9) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.13 168 421 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.43 178 721 N.D. (#) = qualifier out of range (m) = manual integration 12573.D GCMS0531.M Tue Jun 04 11:49:45 2002 Page 1

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GCMS analysis results for sample AE12570, June 2002 · Box DEP Box 15

NYC-WTC_000014680

Laboratory report documenting GCMS analysis of sample AE12570 conducted on June 7, 2002, including surrogate recovery data.

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