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GCMS analysis results for sample AE12574, June 2002

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Laboratory report documenting GCMS analysis of sample AE12574 conducted on June 7, 2002, including surrogate recovery data.

NYC-WTC_000014720–000014728

Folder label: “GCMS X 5/28/02 A 6/4/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) ' Data File C:\HPCHEM\1\DATA\JUNO 302\12574.D Vial: 25 Acq On 4 Jun 2002 8:54 am Operator: Sample gc/ms scan 5/28 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jun 4 11:50 2002 Quant Results File: GCMS0531.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 09:43:55 2002 Response via : Initial Calibration DataAcq Meth : GCMS0531

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.07 152 496144 40.00 ug/1 0.00 10) Naphthalene-d8 15.69 136 1994397 40.00 ug/1 -0.02 17) Acenaphthene-diO 20.99 164 946357 40.00 ug/1 0.00 30) Phenanthrene-diO 25.43 188 1470703 40.00 ug/1 0.00 38) Chrysene-dl2 33.47 240 806248 40.00 ug/1 -0.04 44) Perylene-dl2 37.65 264 469120 40.00 ug/1 -0.03 System Monitoring Compounds 28) TCMX 23.13 209 196816 30.06 ug/L -0.02 Spiked Amount 40.000 Recovery 75.15% Target Compounds Qvalue 2) N-nitrosodimethylamine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3“Dichlorobenzene 12.06 146 544 N.D. 5) 1,4-Dichlorobenzene 12.06 146 544 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 • N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.76 128 370 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Ac enaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.49 149 496 N.D. 26) 4-Chlorophenylphenylether 23.13 204 1285 N.D. 2 7) Fluorene 0.00 166 0 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.13 168 454 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.43 178 462 N.D. (#) = qualifier out of range (m) = manual integration 12574.D GCMS0531.M Tue Jun 04 11:50:34 2002 Page 1

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NYC-WTC_000014722Source: NYC Law Department, mirrored locally

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