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GCMS analysis results for sample AE12673, June 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12673 conducted on June 6, 2002.

NYC-WTC_000014996–000015005

Folder label: “GCMS X 5/30/02 A 6/1/02

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NYC 9/11 Public Portal Document LSC Area Percent Report J Data File C:\HPCHEM\l\DATA\MAY3102\12673.D Vial: 18 Acq On 1 Jun 2002 4:43 am Operator: Morgan Sample gc/ms scan 5/30 . Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P 2** Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) *e- Title : 209 625/TdLP calibration table Smoothing : OFF Filtering: 5 Sampling 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 5.216 15 19 40 rVB 19388 47271 1.18% 0.212% 2 8.062 325 329 333 rBV 47271 104954 2.62% 0.471% 3 12.064 759 765 782 rBV 1181530 2850100 71.13% 12.789% 4 15.690 1153 1160 1175 rBV 1791517 3853006 96.16% 17.289% 5 20.987 1730 1737 1749 rBV 1823550 3945298 98.47% 17.703% 6 23.136 1962 1971 1981 rBV 1039961 2223368 55.49% 9.977% 7 25.431 2213 2221 2231 rBV2 1783449 4006666 100.00% 17.978% 8 27.404 2431 2436 2441 rBV 21592 43067 1.07% 0.193% 9 33.473 3090 3097 3119 rBV2 1276361 2994581 74.74% 13.437% 10 37.659 3544 3553 3566 rBV2 743794 2217645 55.35% 9.951%

Sum of corrected areas: 22285956 12673.D GCMS0531.M Mon Jun 03 11:44:52 2002

NYC-WTC_000015001

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NYC-WTC_000015001Source: NYC Law Department, mirrored locally

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