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GCMS analysis results for sample AE12677, June 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12677 conducted on June 6, 2002.

NYC-WTC_000015027–000015035

Folder label: “GCMS X 5/30/02 A 6/1/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File C:\HPCHEM\1\DATA\MAY3102\12677.D Vial: 22 Acq On 1 Jun 2002 8:39 am Operator: Morgan Sample gc/ms scan 5/30 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P 2** Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) ses Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline -drop else tangent > Peak separation: 5 Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.064 325 329 332 rBV 41440 84778 2.27% 0.409% 2 12.067 759 765 782 rBV 1073769 2656766 71.23% 12.825% 3 15.693 1154 1160 1178 rBV 1696677 3608997 96.76% 17.422% 4 20.990 1730 1737 1752 rBV 1779907 3690508 98.94% 17.815% 5 23.129 1961 1970 1979 rBV 933198 1968738 52.78% 9.504%

6 25.424 2211 2220 2232 rBV2 1710044 3729949 100.00% 18.006% 7 33.475 3090 3097 3111 rBV2 1198232 2817902 75.55% 13.603% 8 37.652 3544 3552 3571 rBV2 731128 2157692 57.85% 10.416%

Sum of corrected areas: 20715330 12677.D GCMS0531.M Mon Jun 03 11:45:48 2002

NYC-WTC_000015032

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NYC-WTC_000015032Source: NYC Law Department, mirrored locally

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