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GCMS analysis report sample AE12098, June 2002

Machine-extracted title · confidence 95%

GCMS laboratory analysis report for sample AE12098 showing unknown compounds and surrogate recovery data from June 6, 2002.

NYC-WTC_000014883–000014892

Folder label: “GCMS X 5/29/02 A 5/31/02

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Scanned page image, NYC-WTC_000014888
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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\MAY3102\12098.D Vial: 6 Acq On : 31 May 2002 4:53 pm Operator: Morgan Sample : gc/ms scan 5/29 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P 2** *e- Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.071 327 330 332 rBV 21032 39525 1.06% 0.195% 2 8.108 332 334 343 rVB 23727 54476 1.46% 0.268% 3 12.065 759 765 789 rBV 1077280 2594779 69.70% 12.785% 4 15.691 1153 1160 1177 rBV 1631946 3530058 94.82% 17.394% 5 20.988 1730 1737 1750 rBV 1655524 3626234 97.40% 17.868% 6 23.136 1962 1971 1983 rBV 772912 1647859 44.26% 8.120% 7 25.431 2213 2221 2232 rBV2 1666632 3722998 100.00% 18.345% 8 27.405 2431 2436 2442 rBV 57684 105750 2.84% 0.521% 9 33.473 3090 3097 3112 rBV2 1204862 2825613 75.90% 13.923% 10 37.660 3544 3553 3572 rBV2 747544 2147489 57.68% 10.581%

Sum of corrected areas: 20294781 12098.D GCMS0531.M Mon Jun 03 09:34:18 2002

NYC-WTC_000014888

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NYC-WTC_000014888Source: NYC Law Department, mirrored locally

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