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Document / 11 pages

GCMS calibration data AE12095, DEP Labs, May 2002

Machine-extracted title · confidence 100%

Calibration table and internal standard data for sample AE12095 analyzed on May 31, 2002.

NYC-WTC_000014825–000014835

Folder label: “GCMS X 5/29/02 A 5/30/02

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NYC 9/11 Public Portal Document LSC Area Percent Report •Data File : C:\HPCHEM\l\DATA\MAY3002\12096.D Vial: 15 Acq On : 31 May 2002 3:50 am Operator: Morgan Sample : re-ext Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P r' Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) *e- Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal :• TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.068 325 329 331 rBV 35428 71002 1.67% 0.307% 2 8.105 331 333 343 rVB 22528 58917 1.38% 0.255% 3 12.061 759 764 788 rBV 1183993 3054646 71.69% 13.220% 4 15.697 1153 1160 1177 rBV 1909712 4173338 97.94% 18.062% 5 20.994 1730 1737 1758 rBV 1935995 4227037 99.20% 18.294%

6 23.133 1960 1970 1984 rBV 846190 1766785 41.46% 7.646% 7 25.428 2213 2220 2231 rBV2 1940689 4260945 100.00% 18.441% 8 25.566 2231 2235 2247 rVB 16924 51324 1.20% 0.222% 9 33.470 3089 3096 3110 rBV2 1286180 3109730 72.98% 13.458% 10 37.656 3544 3552 3575 rBV2 801558 2332415 54.74% 10.094%

Sum of corrected areas: 23106139 12096.D GCMS0520.M Fri May 31 11:34:53 2002

NYC-WTC_000014830

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NYC-WTC_000014830Source: NYC Law Department, mirrored locally

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