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GCMS calibration data AE11284, DEP Labs, May 2002

Machine-extracted title · confidence 100%

Calibration data for sample AE11284 analyzed using Method 508 on May 17, 2002.

NYC-WTC_000014807–000014817

Folder label: “GCMS X 5/29/02 A 5/30/02

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\MAY3002\12095.D Vial: 14 * Acq On : 31 May 2002 2:51 am Operator: Morgan Sample : re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) *es Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.062 326 329 332 rBV 34166 70719 1.67% 0.306% 2 8.108 332 334 343 rVB 22862 55467 1.31% 0.240% 3 12.065 760 765 785 rBV 1239210 3063934 72.21% 13.249% 4 15.691 1154 1160 1178 rBV 1936062 4162900 98.12% 18.001% 5 20.988 1731 1737 1753 rBV 1949216 4227046 99.63% 18.279% 6 23.127 1962 1970 1980 rBV 816710 1732019 40.82% 7.490% 7 25.431 2214 2221 2231 rBV2 1914218 4242815 100.00% 18.347% 8 25.569 2231 2236 2246 rVB 17132 50013 1.18% 0.216% 9 33.473 3090 3097 3113 rBV2 1351081 3155744 74.38% 13.646% 10 37.659 3544 3553 3573 rBV2 796999 2365088 55.74% 10.227%

Sum of corrected areas: 23125745 12095.D GCMS0520.M Fri May 31 11:34:36 2002

NYC-WTC_000014812

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NYC-WTC_000014812Source: NYC Law Department, mirrored locally

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