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GCMS calibration table data, DEP Labs, May 2002

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Calibration table data for GCMS analysis including internal standards and response factors from May 31, 2002.

NYC-WTC_000014771–000014780

Folder label: “GCMS X 5/29/02 A 5/30/02

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NYC 9/11 Public Portal Document LSC Area Percent Report • Data File : C:\HPCHEM\1\DATA\MAY3002\11284.D Vial: 11 Acq On : 30 May 2002 11:55 pm Operator: Morgan Sample : re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.063 326 329 347 rBV 33562 100852 2.25% 0.419% 2 12.065 760 765 795 rBV 1299771 3221889 71.75% 13.393% 3 15.691 1154 1160 1177 rBV 1998194 4384315 97.63% 18.225% 4 20.988 1731 1737 1758 rBV 2043596 4490706 100.00% 18.668% 5 23.137 1959 1971 1983 rBV 843589 1823473 40.61% f- 7.580% 6 25.432 2213 2221 2231 rBV2 2006807 4480203 99.77% 18.624% 7 25.569 2232 2236 2244 rVB 17177 46324 1.03% 0.193% 8 33.474 3090 3097 3115 rBV2 1399768 3183374 70.89% 13.233% 9 37.660 3544 3553 3571 rBV2 773298 2325001 51.77% 9.665%

Sum of corrected areas: 24056137 11284.D GCMS0520.M Fri May 31 11:33:55 2002

NYC-WTC_000014776

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NYC-WTC_000014776Source: NYC Law Department, mirrored locally

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