GCMS sample results AE11284, DEP Labs, June 2002

NYC 9/11 Public Portal Document LSC Area percent Report Data File : C:\MSDCHEM\1\DATA\020516\11284.D Vial: 12 Acq On : 16 May 2002 8:14 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) 5 * 6* Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 0.5 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 6.158 515 524 565 rBV 627103 1257533 39.88% 5.995% 2 7.597 761 769 775 rBV6 8833 19978 0.63% 0.095% 3 7.932 819 826 839 rBV2 18494 41883 1.33% 0.200% 4 8.984 999 1005 1015 rVB6 8003 21512 0.68% 0.103% 5 9.760 1126 1137 1147 rBV2 18670 52790 1.67% 0.252% 6 9.865 1147 1155 1162 rVB5 14178 34073 1.08% 0.162% 7 9.977 1168 1174 1178 rBV3 8776 18124 0.57% 0.086% 8 10.024 1178 1182 1193 rVB4 11492 25748 0.82% 0.123% 9 10.177 1201 1208 1219 rW5 9527 27546 0.87% 0.131% 10 10.277 1219 1225 1243 rVB4 11876 33477 1.06% 0.160%

11 10.535 1257 1269 1273 rBV7 7017 23002 0.73% 0.110% 12 10.794 1305 1313 1326 rVB 26778 65490 2.08% 0.312% 13 11.123 1359 1369 1382 rVB 45038 116349 3.69% 0.555% 14 11.370 1400 1411 1433 rVB 904711 2290119 72.62% 10.917% 15 11.622 1448 1454 1471 rVB7 12332 48422 1.54% 0.231% 16 11.804 1477 1485 1498 rVB4 17062 52252 1.66% 0.249% 17 12.515 1594 1606 1613 rBV5 5764 19377 0.61% 0.092% 18 12.627 1614 1625 1632 rBV2 10852 27508 0.87% 0.131% 19 12.786 1643 1652 1656 rBV9 12734 36536 1.16% 0.174% 20 13.038 1683 1695 1709 rBV8 11312 48253 1.53% 0.230% 21 13.156 1709 1715 1725 rVB7 9216 25994 0.82% 0.124% 22 13.367 1738 1751 1760 rBV7 11564 52614 1.67% 0.251% 23 13.455 1760 1766 1785 rVB9 12410 46046 1.46% 0.220% 24 13.649 1787 1799 1806 rBV8 16901 49717 1.58% 0.237% 25 14.213 1887 1895 1897 rBV4 12677 27460 0.87% 0.131% 26 14.266 1897 1904 1917 rVB5 47911 135191 4.29% 0.644% 27 14.548 1946 1952 1958 rBV5 7123 20512 0.65% 0.098% 28 14.619 1959 1964 1970 rW5 6896 17265 0.55% 0.082% 29 14.707 1973 1979 1996 rVB5 12242 42560 1.35% 0.203% 30 15.265 2062 2074 2076 rBV9 10562 28783 0.91% 0.137%

31 15.394 2089 2096 2103 rBV8 6650 21712 0.69% 0.104% 11284.D SCAN020507.M Fri May 17 13:06:36 2002 Page 1

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