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GCMS analysis results for sample AE12571, June 2002

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Laboratory report documenting GCMS analysis of sample AE12571 conducted on June 7, 2002, including surrogate recovery data.

NYC-WTC_000014690–000014699

Folder label: “GCMS X 5/28/02 A 6/4/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File C:\HPCHEM\1\DATA\JUNO3O2\12571 .D Vial: 22 Acq On 4 Jun 2002 5:55 am Operator: Sample gc/ms scan 5/28 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jun 4 11:47 2002 Quant Results File: GCMS0531.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 09:43:55 2002 Response via : Initial Calibration DataAcq Meth : GCMS0531

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.07 152 462812 40.00 ug/1 0.00 10) Naphthalene-d8 15.70 136 1842530 40.00 ug/1 -0.02 17) Acenaphthene-diO 20.99 164 882311 40.00 ug/1 0.00 30) Phenanthrene-diO 25.43 188 1362447 40.00 ug/1 0.00 38) Chrysene-dl2 33.47 240 768823 40.00 ug/1 -0.04 44) Perylene-dl2 37.66 264 451601 40.00 ug/1 -0.03 System Monitoring Compounds 28) TCMX 23.13 209 177615 :29.10 ug/L -0.02 Spiked Amount 40.000 Recovery 72.75% Target Compounds Qvalue 2) N-nitrosodimethylamine 5.40 74 267 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 11.97 146 334 N.D. 5) 1,4-Dichlorobenzene 12.11 146 668 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 15.59 180 290 N.D. 15) Naphthalene 15.75 128 1630 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachiorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 20.53 152 329 N.D. 2 3) Acenaphthene 21.08 153 286 N.D. 24) 2,4-Dinitrotoluene 21.33 165 171 N.D. 25) Diethylphthalate 22.49 149 289 N.D. 26) 4-Chlorophenylphenylether 23.13 204 972 N.D. 27) Fluorene 22.63 166 187 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.13 168 589 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 3 3) Hexachiorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.48 178 327 N.D. (#) = qualifier out of range (m) = manual integration 12571.D GCMS0531.M Tue Jun 04 11:48:00 2002 Page 1

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