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GCMS blank results for VOCs, sample AE12535, June 2002

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Laboratory report showing GCMS blank analysis results for volatile organic compounds in sample AE12535 on June 3-4, 2002.

NYC-WTC_000014611–000014619

Folder label: “GCMS X 5/28/02 A 6/4/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\JUN03 02\LBA.D Vial: 13 Acq On 3 Jun 2002 9:01 pm Operator: Sample gc/ms scan 5/28 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jun 4 11:35 2002 Quant Results File: GCMS0531.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 09:43:55 2002 Response via : Initial Calibration DataAcq Meth : GCMS0531

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.07 152 484743 40.00 ug/1 -0.01 10) Naphthalene-d8 15.69 136 1925772 40.00 ug/1 -0.02 17) Acenaphthene-diO 20.99 164 922716 40.00 ug/1 -0.01 30) Phenanthrene-diO 25.42 188 1422874 40.00 ug/1 -0.01 38) Chrysene-dl2 33.48 240 804882 40.00 ug/1 -0.03 44) Perylene-dl2 37.65 264 466567 40.00 ug/1 -0.03

System Monitoring Compounds 28) TCMX 23.14 209 192117 30.09 ug/L -0.01 Spiked Amount 40.000 Recovery 75.22% Target Compounds Qvalue 2) N-nitrosodimethylamine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 11.97 146 460 N.D. 5) 1,4-Dichlorobenzene 12.07 146 1203 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2’-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 13.47 117 174 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.75 128 624 N.D. 16) Hexachlorobutadiene 16.31 225 457 N.D. 18) Hexachiorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.48 149 260 N.D. 26) 4-Chlorophenylphenylether 23.13 204 1303 -N.D. 27) Fluorene 0.00 166 0 N.D. 2 9) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 3 3) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.44 178 525 N.D. (#) = qualifier out of range (m) = manual integration LBA.D GCMS0531.M Tue Jun 04 11:35:28 2002 Page 1

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