Gas chromatography mass spectrometry results for sample AE12324 including surrogate recovery data analyzed on June 7, 2002.
NYC-WTC_000014303–000014329Folder label: “GCMS X 5/24/02 A 5/29/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document UDLCLy DCaLCil tompOunC RepOLL
Data File : C:\MSDCHEM\1\DATA\052902\12324.D Vial: 12 Acq On : 29 May 2002 7:03 pm Operator: McLean Sample : gc/ms scan 5/24 fb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L
Peak Number 11 l-Buten-3-yne, 2-chloro- Concentration Rank 9 RT. EstConc Area Relative to ISTD R.T. 4.43 0.78 ug/L 522603 1,4-Dichlorobenzene-d4 9.90 Hit# of . 5 Tentative ID MW MolForm CAS# Qual 1 1-Buten-3-yne, 2-chloro- 86 C4H3C1 017712-36-6 7 2 Crotonic acid 86 C4H602• 003724-65-0 5 3 Isocrotonic acid 86 C4H6O2 000503-64-0 • 4 2-Butenoic acid, (E) - 86 C4H602 000107-93-7 4 Abundance Scan 229 (4.425 min): 12324.D (-225) (-) m/z 86.00 1 .00% 83
5000 49 39 1 42 82 4.00 4.20 4.40 4.60 4.80 Of ”I''“I'" 'I ‘‘ “ I ‘“ I‘I““I ‘“ ‘I''I'' amrl| -mp-rrTp-rr m/z 49.10 27.17% miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #34744:1-Buten-3-yne, 2-chloro- 51 83
5000 1*1*1’* l-r-|- l ■ i , pi i i i | > 1 > 4.00 4.20 4.40 4.60 4.80 m/z 87.10 19.20% 60 niz-> 99 7 01 . , | I I . . ! . . . . | . . . . I . , . I | I I I I | I I ! | | I I I > | I 1 1 I | I | ! —mmmpmmt 5 10 15 20 25 3035404550556065 70 75 80859095 M Abundance #116766: Crotonic acid 41 85
4.00 4.20 4.40 4.60 4.80 5000 m/z 88.00 17.93% 69
m/z-> 01 +13418,.241 15 13134 27 1 5053 5760 66 72 38
5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 m 45
—mmpm 80 85 90 95 "h"mmirpau. Abundance #34646: Isocrotonic acid 39 83 4.00 4.20 4.40 4.60 4.80 m/z 39.10 17.75% 5000 68
27 .245 71
miz-> 0 +7AAFFAHFH431.,3§ + . 53 5760 H 5 10 15 20 25 30 35 40 45 50 556065 70 75 80859095 '" i" ” i ‘1 ■
4.00 TT 4.20 4.40 TII 4.60 4.80
12324.D 052202.M Mon Jun 03 10:52:14 2002 Page 14
NYC-WTC_000014321
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NYC-WTC_000014214
Gas chromatography mass spectrometry results for sample AE12320 including surrogate recovery data analyzed on June 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014189
Gas chromatography mass spectrometry results for sample AE12288 including surrogate recovery data analyzed on June 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014260
Gas chromatography mass spectrometry results for sample AE12322 including surrogate recovery data analyzed on June 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014237
Gas chromatography mass spectrometry results for sample AE12321 including surrogate recovery data analyzed on June 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014004
GCMS analysis results for sample AE12287 dated June 4, 2002, documenting unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014154
Laboratory report documenting gas chromatography-mass spectrometry analysis of a method blank (AE12288) for volatile organic compounds on June 3, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014552
Laboratory report showing GCMS analysis results for sample AE12533 including surrogate recovery data on June 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013921
GCMS analysis report for sample AE11602 dated June 4, 2002, documenting unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015410
Gas chromatography-mass spectrometry analysis report for sample AE12743 detecting unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015777
Gas chromatography-mass spectrometry results for sample AE12763 analyzed on June 12, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014033
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12327 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014433
Laboratory report showing GCMS analysis results for sample AE12477 including surrogate recovery data on June 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000014149
Laboratory log listing the sequence of samples and calibration standards processed by GCMS on May 24 and May 28, 2002.
Filed in the same folder
NYC-WTC_000014150
Fragmented document header from the DEP Box 15 archive containing metadata for environmental testing records dated late May 2002.
Filed in the same folder
NYC-WTC_000014154
Laboratory report documenting gas chromatography-mass spectrometry analysis of a method blank (AE12288) for volatile organic compounds on June 3, 2002.
Filed in the same folder
NYC-WTC_000014177
Calculated reference values and recovery percentages for organic compound analysis using gas chromatography-mass spectrometry with all results at or above 2.0 ug reporting limit.
Filed in the same folder
NYC-WTC_000014185
Laboratory report showing reference calculations for volatile organic compounds in sample AE12288 analyzed on June 3, 2002.
Filed in the same folder