GCMS analysis results for sample AE12475, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052802\12475.D vial: 13 Acq On : 29 May 2002 12:04 am Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Piperidine Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 3.99 0.99 ug/L 642780 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Piperidine 85 C5H11N 000110-89-4 9 2 Piperidine 85 C5H11N 000110-89-4/9 3 Piperidine 85 C5H11N 000110-89-/ 9 4 Krypton 84 Kr 007439-90-9 5 Abundance Scan 155 (3.990 min): 12475.D (-154) (-) m/z 51.10 100.00%

P 51 84

5000 43 47 70 35 40 58 3.60 3.80 4.00 4.20 4.40

iz-> 04T" 5 i'••• । • •', । -4 ‘I‘ "i>•■■ । ■i H ■ ■ i •1 “ i ‘ ■ 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 “ ■ i ■ ■ “ i ■ m/z_ 84.00 98.01% Abundance #116576: Piperidine 84

56 5000 14 *** ’ 11/441’17711’1’14" 28 3.60 3.80 4.00 4.20 4.40 m/z , 86.0 0 63.68% 15 32 38 | 4144 50531 677° 80 04’it 111 । > > >' 111" 1111111 1111111il11111111111111111111 TTPHTTH miz-> 5 10 15 20 253035404550556065 70 75 80859095 Abundance , #33820: Piperidine 84

3.60 3.80 4.00 4.20 4.40 5000 57 m/z 43.10 43.59% 29 44

01 .......................... 41 5154 TTTHT 67 70 I 79 TI 11 | I 1 I I I H I I | I I I I | I I I pTp hd MAmakta z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #116601: Piperidine 84 3.60 3.80 4.00 4.20 4.40 m/z 84.95 41.88%|

5000 56 29 .44 70

n/z—> 0 ---2635315051TMPmmt 63 67 । 76 80,, A7 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.60 3.80 4.00 4.20 4.40

12475.D 052202.M Thu May 30 10:43:26 2002 Page 8

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