GCMS analysis results, sample AE12532, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052902\12532.D Vial: 23 Acq On : 30 May 2002 4:00 am Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 4 Piperidine Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 3.85 0.49 ug/L 320714 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qua

1 Piperidine 85 C5H11N 000110-89-4 9 2 Piperidine 85 C5H11N 000110-89-4/9 3 Piperidine 85 C5H11N 000110-89-4 9 4 Piperidine, 1,1'-dithiobis- 232 C10H20N2S2 010220-20-9 9 Abundance Scan 131 (3.849 min): 12532.D (-130) (-) m/z 47.05 TOO.00% 47 84

5000

36 4043 87 ■ ‘ ■ i ■ ■ ■ • i ■ ' • ■ I 1 ' 1 1 i 1 1 ' 3.60 3.80 4.00 4.20 0- " i1 ■ “ i' ■ ■ ■ i ■" ‘ i ■ • ■ ■ i" " i • ■ ■ ■ i • ' ‘ I “ ‘ ' I ' m/z 84.00 71.07% miz-> 5 10 15 2025303540 45 50556065 70 75 80859095 Abundance #33820: Piperidine 84

50)0 57 ■ ■ ■ ■ । ■111111 ■ i'11 ■ i ■1 ■ 29 44 3.60 3.80 4.00 4.20 m/z 85,00 36.45% 41 70 0 1518 • j i • *»j. • < * | “1 * —2 323538 l. »■■■5154 In1 i| 111. j. 67 | 79 H 1111 H 11 m-j» r 1111 > > H mfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #116576: Piperidine 84

wlnl 56 3.60 3.80 4.00 4.20 50001 28 44 41 70 15 32 38 I 50531 67 1 80 0: 11111111111 fn 111111.11 HH PtH —Tm m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #116600: Piperidine 1 ' I ' ‘ ‘ I ' ‘ I ‘ ‘ ' I ‘ ' 84 3.60 3.80 4.00 4.20 m/z ___ 43.05 16.17% 5000 28 56 44 41 15 2 70 A miz—> 0- *711110111112 1.3534 5053 67 1 80 71 ■■ 11 H 1 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ‘ ' I ' ‘ ' I • ' ‘ ■ I ‘ ' I ‘ ‘ 3.60 3.80 4.00 4.20

12532.D 052202.M Mon Jun 03 11:44:16 2002 Page 6

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