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GCMS analysis results for sample AE12474, June 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12474 conducted on June 4, 2002.

NYC-WTC_000014102–000014124

Folder label: “GCMS X 5/24/02 A 5/28/02

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NYC 9/11 Public Portal Document Llorary searcn compound Keport

Data File : C:\MSDCHEM\l\DATA\052802\12474.D Vial: 12 Acq On : 28 May 2002 11:15 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan *** Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 9 Cyclotrisiloxane, hexamethyl- Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 5.37 0.28 ug/L 169595 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotri siloxane, hexamethyl- 222 C6H1803Si3 000541-05-9 9/ 2 Cyclotrisiloxane, hexamethyl- 222 C6H1803Si3; 000541-05-9 9 3 Benzenamine, 4-bromo-2-chioro- 205 C6H5BrClN 038762-41-3 /5 4 2-Methyl-6-(5-methyl- 2-thiazolin... 207 C10H13N3S 1000225-39-^ 5 Abundance Scan 389 (5.365 min): 12474.D (-384) (-) m/z 207.00 100/00% 207

5000 86 96 191 48 58 500 5.20 5.40 5.60 5.80

miz-> 0- .......... 0 20 l,60.....80I .),100 40 120 140 160 180 200 L’ ‘ i m/z 86.00 37.76% Abundance #126480: Cyclotrisiloxane, hexamethyl- 207

5000 500 5.20 5.40 5.60 5.80 36 m/z 208.00 34.88% . 133 . _ j— — 191 45 75 86. 0- 28 61 i ■1 ■ ■ i ■11 ■ i 7 ■1 * T111','‘ r ■ ‘r1 106 119 . L 147 163 177 (_ __ i1..... FTT' 111 I ' ' 1 ' r1 1 1 1 1 1 1 T"' I " * ‘ I niz-> 0 20 40 60 80 100 120 140 160 180 200 Abundance #84874: Cyclotrisiloxane, hexamethyl- 207

5.00 5.20 5.40 5.60 5.80 5000 m/Z 84.00 24.47%

96 0- 4 15 29 _ 45 _ 61 , 75 85 , f 119 123 147 163 177 111 1B.I miz-> 0 20 40 60 80 100 120 140 160 180 200 Abundance #84854: Benzenamine, 4-bromo-2-chloro- 1 * । ‘ ‘ ‘ i * ' 207 5.00 5.20 5.40 5.60 5.80 m/z 96.10 23.59% 90 5000 63 126 44 , - 73 0 ■ ’iK 7 i11 l. 83 115 M,, 143153 169179 TTIB 4— i ■* 1 ’ * I ' d* i 1 1 • mz—> 0 20 40 60 80 100 120 140 160 180 200 5.00 5.20 5.40 5.60 5.80

12474.D 052202.M Thu May 30 10:43:00 2002 Page 12

NYC-WTC_000014118

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NYC-WTC_000014118Source: NYC Law Department, mirrored locally

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