GCMS analysis results for sample AE12473, June 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12473 conducted on June 4, 2002.

NYC-WTC_000014079–000014101

Folder label: “GCMS X 5/24/02 A 5/28/02”

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NYC 9/11 Public Portal Document JLJLCLy DCaLtil ttpOul RCPOLL

Data File : C:\MSDCHEM\1\DATA\052802\12473.D Vial: 11 Acq On : 28 May 2002 10:26 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 12 Cyclopentasiloxane, decamet... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 12.37 0.26 ug/L 215329 Napthalene-dS 13.39 Hit# of 5 Tentative ID MW MolForm CAS# Qua: 1 Cyclopentasiloxane, decamethyl- 370 C10H30O5S15 000541-02-6 778 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 50 3 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3S13 010538-85-9 17 4 Benzeneethanamine, N-[ (pentaf luo. . . 563 C24H34F5NO3Si3 055429-13-5 12 Abundance Scan 1582 (12.375 min): 12473.D (-1575) (-) m/z 73.10 ¥00.00% 73

5000 267 355 / ‘I I ‘ ’ 1 1 * 45 154 191 12.00 12.20 12.40 12.60 12.80 p-rTTpH-TTp-rrTp-rTTp-rKkmmmmmmmmmm .1 r. 0'rp-m-rm T*—ma"ugmuap3r m/z 267.00 40.81% n/z-> 20 40 60 80 100 120140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #115315: Cyclopentasiloxane, decamethyl- 73 355 267 5000 1200 12.20 12.40 12.60 12.80 m/z 355.00 28.21% 45 207 249 I 323 0 A..).. A,.., mte I1"1I“' iz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #115273: Cyclopentasiloxane, decamethyl- 73 • i ■ ■ ‘ ' i ■ T-pn-r-rp-r 12.00 12.20 12.40 12.60 12.80 5000 267 m/z 356.00 8.79% 355 45 2811 96 115133 165,193 22341 423 2 4 0 11 ■1" i ’ ■ “ i ■ ■n i ■ ■ U—mpTumggu miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 3(X) 320 340 360 380 Abundance #115313: Phenethylamine, N-methyl-beta.,3,4-tris(trimethy... 1 i ■ ' ■ ■ i ■ ■ i 1 1 • • i 17 1 1 r 1 73 12.00 12.20 12.40 12.60 12.80 m/z 267.90 8.39%

5000 355 44 l.. ..,u93 130147 OTTTm*ngmmmmmmmmu . 1?3 220237 267 294_____ | 384 n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 12.00 12.20 12.40 12.60 12.80

12473.D 052202.M Thu May 30 10:42:26 2002 Page 14

NYC-WTC_000014097

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GCMS analysis results for sample AE12474, June 2002 · Box DEP Box 15

NYC-WTC_000014102

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12474 conducted on June 4, 2002.

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