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GCMS analysis results for sample AE12473, June 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12473 conducted on June 4, 2002.

NYC-WTC_000014079–000014101

Folder label: “GCMS X 5/24/02 A 5/28/02

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NYC 9/11 Public Portal Document ULJLCLX DCaLtii ~ILpUULIU RCPOLL

Data File : C:\MSDCHEM\l\DATA\052802\12473.D Vial: 11 Acq On : 28 May 2002 10:26 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan **** Library : C:\DATABASE\NIST98.L

Peak Number 10 Azetidine, 1-nitroso- Concentration Rank 15 R.T. EstConc Area Relative to ISTD R.T. 5.20 0.21 ug/L 129147 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qua.

1 Azetidine, 1-nitroso- 86 C3H6N20 015216-10-1 4 2 Imidazol, 4-fluoro- 86 C3H3FN2 030086-17-/ 2 3 Borane, trifluoro- 68 BF3 007637-07-2 2 4 2-Chloroethanol 80 C2H5C1O 000107-07-3 2 Abundance Scan 361 (5,200 min): 12473.D (-359) (-) m/z 49.10 L00.00% 43 86

5000

ERosseli" 82 41 37 4.80 5.00 5.20 5.40 5.60

m/z-> 0-” " i'■" i““i ■" 'i"i“ “ I‘ 4X Hmmmm 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 T 1" I' " ‘ I •

Abundance #734: Azetidine, 1-nitroso- 3b

41 5000 86 4.80 5.00 5.20 5.40 5.60 55 44 m/z 84.00 62.43%

nz-> Or m 0 i “' ‘i1' “ I ‘ ■r■ — 1 3& 5 10 15 20253035404550556065 70 75 80859095 58 4+ — 52

Abundance #34862: Imidazol, 4-fluoro- 85

4.80 5.00 5.20 5.40 5.60 5000 m/z 48.00 26.87% 59 0- Ppp m/z-> 0 5 10 15 20 25 30 35 40 45 50 55 60 70 75 80 85 90 95 Abundance #12321: Borane, trifluoro- 49 4.80 5.00 5.20 5.40 5.60 m/z 81.90 25.67% 5000

68 0- 11 19 Kn1puuan —30—Gn——38nu———naTm TOTTmLTTPTTTTTTTTTTT n/z—> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 4.80 5.00 5.20 5.40 5.60

12473.D 052202.M Thu May 30 10:42:25 2002 Page 12

NYC-WTC_000014095

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NYC-WTC_000014095Source: NYC Law Department, mirrored locally

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