GCMS analysis results for sample AE10061, May 2002

NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\l\DATA\020507\10061.D Vial: 25 Acq On 8 May 2002 11:46 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan ' Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 Hydroxylamine, 0-pentyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.01 0.61 ug/1 46358 1,4-Dichlorobenzene-d4 11.38

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hydroxylamine, 0-pentyl- 103 C5H13NO 005963-74-6 10 2 Azetidine, /-methyl- 71 C4H9N 004923-79-9 9 3 Furan, 2, - dihydro- 70 C4H60 001708-29-8 9 4 Pentane, / , 3,4-trimethyl- 114 C8H18 000565-75-3 9 Abundance / Scan 329 (5.012 min): 10061.D (-321) (-) m/z 43.10 100.00% / 43 A 71

5000 55 pMhaononAs Wit — ——————— 38 67 4.60 4.80 5.00 5.20 5.40 I I I I I I I I I ■ I TTAH — । ” "i"" i" m/z 41.10 70.85% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #4171: Hydroxylamine, O-pentyl- 43

anaAaAannudd WN 5000 4.60 4.80 5.00 5.20 5.40 55 71 m/z 71.10 66.94% 38 86 103 1 Pp-H—M4i । ri ri rr " i ■ "' r " ' r " ' i " " I " " r " 11 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #119: Azetidine, 1 -methyl- 23 A iBik 1 1 1 1 ' 42 4.60 4.80 5.00 5.20 5.40 5000 m/z 69.10 62.99% 56 71

m/z-> "‘IT .I I. 1 mm 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 ■ i"1111

Abundance #108475: Furan, 2,5-dihydro- - -A--AAAAA- 41 4.60 4.80 5.00 5.20 5.40 70 m/z 55.10 37.65% 5000

m/z—> i ■ ■ ■1 r " ■ i 39 i.I I 11 i । 50 55 i | | i ri *!' i ri i । ■ i i । joT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 1'11111" I " 111'' " I " 1' 111111" '' I' TC)’ ' — 4.60 4.80 5.00 5.20 5.40

10061 .D SCAN020507.M Tue May 14 08:46:39 2002 Page 3

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