GCMS data file header for May 24-28, 2002

NYC 9/11 Public Portal Document Llprary searcn compound Report

Data File : C:\MSDCHEM\1\DATA\052802\524LB.D Vial: 3 Acq On : 28 May 2002 3:56 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library- : C:\DATABASE\NIST98.L

Peak Number 5 1-Pyrrolidineethanamine Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 4.23 0.36 ug/L 236498 1,4-Dichlorobenzene-d4 9.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1- Pyrrol idineethanamine 114 C6H14N2 007154-73-8 9 2 3-Amino-s-triazole 84 C2H4N4 000061-82-5 4 3 Thiophene 84 C4H4S 000110-02-1 4 4 Thiophene 84 C4H4S 000110-02-1 4 Abundance Scan 196 (4.231 min): 524LB.D (-193) (-) m/z 86.00 100.00% 86

5000 51 73 42 i ■ ‘ ‘ • i • ■ ■ ■ i ■ ■ ■ ' i 1 1 1 ' 1 1 1 1 58 3.80 4.00 4.20 4.40 4.60 m/z-> 01 ' ‘ i ‘ ■ i ■ ■ ■ • i ■ H44 ......................... I ‘ I 1 ■ ' • i ■ ' ■ ■ i ‘ 90 100 110 120 m/z 84.00 94.31% 10 20 30 40 50 60 70 80 Abundance #33571: 1-Pyrrolidineethanamine 84 42 5000 3.80 4.00 4.20 4.40 4.60 55 m/z 51.00 42.55% 70 01 TTI ■ 18 +11 1+784 ... 9,111771].... . m/z-> 10 20 30 40 50 60 701 80 90 100 110 120 Abundance #209:3-Amino-s-triazole 23

84 3.80 4.00 4.20 4.40 4.60 ‘ 5000 m/z 73.10 40.78% 57 43 18 68 77 0! - I 1+) ■ ' I] 364 50 „ i । । I ।11 ■ i • i * ‘ * i ‘ 1 * 1 i 1 n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #116584: Thiophene • • i ‘ 1 ■ ■ i ■ • ■ 84 3.80 4.00 4.20 4.40 4.60 58 m/z 42.10 36.47% 45 5000 39

26 32 il 69 01 11 r11 ■ M 1 l 11'111 # -4L ----- n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 3.80 4.00 4.20 440 4.60'

524LB.D 052202.M Thu May 30 10:44:15 2002 Page 8

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