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GCMS analysis results for sample AE11421, May 2002

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Laboratory report showing GCMS results for sample AE11421 analyzed on May 30, 2002.

NYC-WTC_000025447–000025463

Folder label: “GCMS X 5/16/02 A 5/20/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052002\11421.D Vial: 11 Acq On : 20 May 2002 9:26 pm Operator: Mclean Sample : 5/16 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 4 3-Thio-1,2,4-triazin-3,5(2H... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 5.08 0.26 ug/L 205994 1,4-Dichlorobenzene-d4 9.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Thio-1,2,4-triazin-3,5(2H,4H)-... 129 C3H3N30S 1000213-20-1 9 2 Pyridine-3,4-dicarbonitrile 129 C7H3N3 001633-44-9 7 3 Thiophene, 2-nitro- 129 C4H3NO2S 000609-40/5 7 4 l-Methyl-3-nitropyrazole 127 C4H5N3O2 054210-32-1 5 Abundance Scan 341 (5.083 min): 11421 .D (-336) (-) m/z 128.90 100.00% 129

5000 .................... ,................... 48 81 93 1 1 1 1 I 1 ' 1 1 I ' 1 1 1 I ' 1 ' 1 I 1 1 ' 208 4.80 5.00 5.20 5.40 0- 35 in, '58 ■ ' i ' 1|I II III|........I.................. ■'i1 ■ 1 1 1 ■ i ' ■ 1 ' i 1 1 1 ' i ' ■ ■ 1 i 1 IrrI i ... । . - m/z 126.90 74.26% mfe-> 20 40 60 80 100 120 140 160 180 200 Abundance #58194: 3-Thio-1,2,4-triazin-3,5(2H,4H)-dione 42 129

5000 60 4.80 5.00 5.20 5.40 m/z 130.90 22.04% 71 86 0- 1 1 i ■ ■ TTI 7l,,p,,191 113. n m/z-> 20 40 60 80 100 120 140 160 180 200 Abundance #58358: Pyridine-3,4-dicarbonitrile 129

4.80 5.00 5.20 5.40

u 5000 102 m/z 48.05 17.14% 51 75 26 — I 38 , 62 89 । miz-> 0- , , i , | III ■ th , ill 20 40 Larihl 60 ' Ilt80 7100ill 120 140 160 180 200 Abundance #58233: Thiophene, 2-nitro- 129 4.80 5.00 5.20 5.40 m/z 92.90 11.94% 45 55 5000 99 71 83 113 0 ......... ll p, Il , ,, T 1 . .. . I ' 1 1 ' T 1 1 I ' , ii II /z-> 20 40 60 80 100 120 140 160 180 200 4.80 5.00 5.20 5.40

11421.D 050102.M Thu May 23 10:48:25 2002 Page 7

NYC-WTC_000025458

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NYC-WTC_000025458Source: NYC Law Department, mirrored locally

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