NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\1\DATA\052002\11421.D Vial: 11
Acq On : 20 May 2002 9:26 pm Operator: Mclean
Sample : 5/16 eh Inst : Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan
Library : C:\DATABASE\NIST98.L
Peak Number 4 3-Thio-1,2,4-triazin-3,5(2H... Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
5.08 0.26 ug/L 205994 1,4-Dichlorobenzene-d4 9.93
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Thio-1,2,4-triazin-3,5(2H,4H)-... 129 C3H3N30S 1000213-20-1 9
2 Pyridine-3,4-dicarbonitrile 129 C7H3N3 001633-44-9 7
3 Thiophene, 2-nitro- 129 C4H3NO2S 000609-40/5 7
4 l-Methyl-3-nitropyrazole 127 C4H5N3O2 054210-32-1 5
Abundance Scan 341 (5.083 min): 11421 .D (-336) (-) m/z 128.90 100.00%
129
5000
.................... ,...................
48 81 93
1 1 1 1 I 1 ' 1 1 I ' 1 1 1 I ' 1 ' 1 I 1 1 '
208 4.80 5.00 5.20 5.40
0-
35 in, '58
■ ' i ' 1|I II
III|........I..................
■'i1 ■ 1 1 1 ■ i ' ■ 1 ' i 1 1 1 ' i ' ■ ■ 1 i 1 IrrI i ... । . - m/z 126.90 74.26%
mfe-> 20 40 60 80 100 120 140 160 180 200
Abundance #58194: 3-Thio-1,2,4-triazin-3,5(2H,4H)-dione
42 129
5000
60 4.80 5.00 5.20 5.40
m/z 130.90 22.04%
71 86
0- 1 1 i ■ ■ TTI 7l,,p,,191 113. n
m/z-> 20 40 60 80 100 120 140 160 180 200
Abundance #58358: Pyridine-3,4-dicarbonitrile
129
4.80 5.00 5.20 5.40
u
5000 102 m/z 48.05 17.14%
51 75
26 —
I 38 , 62 89 ।
miz->
0- , , i , | III ■ th , ill
20 40
Larihl
60
' Ilt80 7100ill 120 140 160 180 200
Abundance #58233: Thiophene, 2-nitro-
129 4.80 5.00 5.20 5.40
m/z 92.90 11.94%
45 55
5000
99
71 83
113
0 ......... ll p, Il , ,,
T 1 . .. . I ' 1 1 ' T 1 1 I ' ,
ii II
/z-> 20 40 60 80 100 120 140 160 180 200 4.80 5.00 5.20 5.40
11421.D 050102.M Thu May 23 10:48:25 2002 Page 7
NYC-WTC_000025458
OCR can misread numbers and units. Confirm readings against the page image before using them.