GCMS analysis report sample AE09682, May 23, 2002

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Data File : C:\MSDCHEM\1\DATA\052102\9682.D Vial: 18 Acq On : 22 May 2002 3:11 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 Toluene Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 4.28 0.85 ug/L 601773 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW' Mol Form CAS# Qual 1 Toluene 92 C7H8 000108-88-3 64 2 Toluene 92 C7H8 000108-88-3 59 3 Toluene 92 C7H8 000108-88-3 53 4 Toluene 92 C7H8 000108-88-3/53 Abundance Scan 204 (4.278 min): 9682.D (-201) (-) m/z 91.05 100/00% 91

5000

39 65 84 4.00 4.20 4.40 4.60 0- ■ ‘ i ‘ ‘ ‘ i ‘ ‘ ‘ ‘ i • ‘ ‘ i • ■ ' 1 I 4558 ....... . ■ ■ 1 i • ■ ■ 1 i ‘ ‘ ■ i 11"i4 ■ i ‘ i m/z 92.10 66.09% miz-> 0 10 20 30 40 50 60 70 80 90 100 Abundance #117281: Toluene 91

5000 . 6.. 4.00 4.20 4.40 4.60 39 51 65 m/z 39.10 17.61%

mfz-> 0- 1 ' ‘ T’ ‘ 1 • i ‘ 0 10 15 27 ' l ■ ■ 1 ' i ■ 20 30 +71,564147864 40 50 60 70 80 90 1 100 Abundance #37326: Toluene 91 I 4.00 4.20 4.40 4.60 5000 m/z 84.00 13.98%

0- 27 39 45 51 60 65 77 86,, 111 1 r1'11 '11,11 ■ ['i'll । ■ 1an 11 ri :’l miz-> 0.10 20 30 40 50 60 70 80 90 100 Abundance #117282: Toluene 91 4.00 4.20 4.40 4.60 m/z 65.00 13.53% 5000

0 —TITTICmm i 27 T 45 51 65 77 86,, n/z—> 0 10 20 30 40 50 60 70 80 90 100 4.00 4.20 4.40 4.60

9682.D 052202.M Wed May 22 11:46:51 2002 Page 9

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