GCMS analysis report sample AE11908, June 4, 2002

NYC 9/11 Public Portal Document_______________________________________________ Library searen compound Report

Data File : C:\MSDCHEM\1\DATA\052202\11908.D Vial: 15 ‘ Acq On : 23 May 2002 1:14 am Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 10 Toluene Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 4.27 1.24 ug/L 771358 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Toluene 92 C7H8 000108-88-3 43 2 Toluene. 92 C7H8 000108-88-3 43 3 Toluene 92 C7H8 000108-88-3/43 4 Toluene 92 C7H8 000108-88-/ 38 Abundance Scan 203 (4.272 min): 11908.D (-199) (-) m/z 91.10 100.00% 91

5000 49 39 . 65 4.00 4.20 4.40 4.60 0- 1 ■ । • 1 1 1 ■ 1 1 11 1 1 '■’■’i1 1 1 1 1,1,1,4.58, .1.1, ....... 44- m/z 92.10 61.90% niz-> 0 10 20 30 4 0 50 60 70 80 90 100 Abundance #117292: Toluene 91

5000 i-r-p-T 4.00 4.20 4.40 4.60 m/z 49.10 31.96% 39 54 65 27 ,| 45 2 57 | 77 86,. i_______ _ 0- 444I ‘ mfe-> 0 10 2030405060 70 8090 100 Abundance #117281: Toluene 91 * ■ • ■ । • i' ■ ■ ■ । ‘ । ■ 4.00 4.20 4.40 4.60

R_ 5000 m/z 51.10 14.63%

39 51 ee65 1 15 27 .. 4 56 ,|. . '77 86, rHi—i , ■ lit 1T—T1*’* । , , .-.LH t 0- * * r* * *11 *4’ • i ‘ *1 * ।1 । mz-> 0 10 20 30 40 50 60 70 80 90 100 Abundance #117282: Toluene ' ‘ • 1 ‘ 1 • *1 ‘ 1 ‘ 1 I ‘ ‘ ‘ ‘ T’ ' ’ * 91 4.00 4.20 4.40 4.60 m/z 39.10 13.86% 5000

m/z-> 0 ..... 27 . 1,45.51. 17.1.77,.88. 0 10 20 30 40 50 60 70 80 90 1

100 MlAfAR,,) 4.00 4.20 4.40 4.60

11908.D 052202.M Tue May 28 12:15:41 2002 Page 13

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