NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\MAY2102\11599.D Vial: 13
Acq On : 22 May 2002 3:12 pm Operator :
Sample : EXTRACTS/20 Inst : 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: May 23 8:17 2002 Quant Results File: GCMS0501.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Wed May 01 10:40:31 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0520
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.14 152 360837 40.00 ug/1 -0.08
10) Naphthalene-d8 15.78 136 1410118 40.00 ug/1 -0.08
17) Acenaphthene-diO 21.09 164 671622 40.00 ug/1 -0.06
30) Phenanthrene-diO 25.53 188 870695 40.00 ug/1 -0.07
38) Chrysene-dl2 33.57 240 487294 40.00 ug/1 -0.09
44) Perylene-dl2 37.79 264 314161 40.00 ug/1 -0.09
System Monitoring Compounds
28) TCMX 23.23 209 130643 39.96 ug/L -0.07
Spiked Amount 10.000 Recovery = 399.60%
Target Compounds
jo)o
Qva lue
2) N-nitroso-dimethyl amine 0.00 74 0 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Di chlorobenzene 0.00 146 0 N.D.
7) 2,2’-oxybi s(1-Chioropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) Isophorone 14.49 82 421 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.83 128 913 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chioronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
22) Acenaphthylene 0.00 152 0 N.D.
2 3) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 22.58 149 988 N.D.
26) 4-Chlorophenyl-phenylether 23.23 204 514 N.D.
27) Fluorene 0.00 166 0 N.D.
2 9) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
31) N-Nitrosodiphenylamine 23.23 168 306 N.D.
32) 4-Bromophenyl-phenylether 0.00 248 0 N.D.
33) Hexachlorobenzene 0.00 284 0 N.D.
3 4) Phenanthrene 25.59 178 1116 N.D.
(#) = qualifier out of range (m) = manual integration
11599.D GCMS0501.M Thu May 23 08:17:54 2002 Page 1
NYC-WTC_000012731
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