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GCMS sample analysis results, AE11599, May 30, 2002

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Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11599.

NYC-WTC_000012729–000012738

Folder label: “GCMS X 5-20-02 A 5-22-02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAY2102\11599.D Vial: 13 Acq On : 22 May 2002 3:12 pm Operator : Sample : EXTRACTS/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 23 8:17 2002 Quant Results File: GCMS0501.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0520

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.14 152 360837 40.00 ug/1 -0.08 10) Naphthalene-d8 15.78 136 1410118 40.00 ug/1 -0.08 17) Acenaphthene-diO 21.09 164 671622 40.00 ug/1 -0.06 30) Phenanthrene-diO 25.53 188 870695 40.00 ug/1 -0.07 38) Chrysene-dl2 33.57 240 487294 40.00 ug/1 -0.09 44) Perylene-dl2 37.79 264 314161 40.00 ug/1 -0.09

System Monitoring Compounds 28) TCMX 23.23 209 130643 39.96 ug/L -0.07 Spiked Amount 10.000 Recovery = 399.60% Target Compounds jo)o Qva lue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Di chlorobenzene 0.00 146 0 N.D. 7) 2,2’-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 14.49 82 421 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.83 128 913 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chioronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.58 149 988 N.D. 26) 4-Chlorophenyl-phenylether 23.23 204 514 N.D. 27) Fluorene 0.00 166 0 N.D. 2 9) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.23 168 306 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.59 178 1116 N.D.

(#) = qualifier out of range (m) = manual integration 11599.D GCMS0501.M Thu May 23 08:17:54 2002 Page 1

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