GCMS sample analysis results, AE11597, May 30, 2002

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Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11597.

NYC-WTC_000012710–000012719

Folder label: “GCMS X 5-20-02 A 5-22-02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAY2102\11597.D Vial: 11 Acq On : 22 May 2002 1:14 pm Operator: Sample : EXTRACT5/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 23 8:08 2002 Quant Results File: GCMS0501.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0520

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) l,4-Dichlorobenzene-d4 12.14 152 396671 40.00 ug/1 -0.07 10) Naphthalene-d8 15.78 136 1551544 40.00 ug/1 -0.07 17) Acenaphthene-dl0 21.09 164 744846 40.00 ug/1 -0.06 3 0) Phenanthrene-dl0 25.53 188 976932 40.00 ug/1 -0.06 38) Chrysene-dl2 33.60 240 566864 40.00 ug/1 -0.06 44) Perylene-dl2 37.83 264 367521 40.00 ug/1 -0.05

System Monitoring Compounds 28) TCMX 23.23 209 143158 39.48 ug/L -0.06 Spiked Amount 10.000 Recovery = -39480% A) S Target Compounds Ovalue 2) N-nitrdso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.84 128 100 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachiorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.58 149 669 N.D. 26) 4-Chlorophenyl-phenylether 23.23 204 671 N.D. 27) Fluorene 0.00 166 0 N.D. 2 9) Azobenzen/ 1,2 -Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.23 168 349 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 0.00 178 0 N.D. (#) = qualifier out of range (m) = manual integration 11597.D GCMS0501.M Thu May 23 08:15:32 2002 Page 1

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GCMS surrogate recovery data, sample AE11573, May 30, 2002 · Box DEP Box 15

NYC-WTC_000012673

Laboratory record from May 30, 2002 documenting the recovery of surrogate standards for sample AE11573.

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