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← Document results/DEP Box 15/525 NOT OVR SAMPLE
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GCMS pesticide analysis results, sample AE11573, May-June 2002

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Laboratory report showing analytical results for pesticides and related compounds with values below method reporting limits.

NYC-WTC_000012615–000012649

Folder label: “525 NOT OVR SAMPLE

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) 4 Data File : C:\MSDCHEM\1\DATA\052902\11311RR.D Vial: 16 * Acq On : 29 May 2002 2:39 pm Operator: Bohlk / Inst 213 Sample : SAMPLE 11311 RE-EXTD 5/23/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Jun 03 15:48:57 2002 Quant Results File: 052802.RES

Quant Method : C:\MSDCHEM\l\5973N\052802.M (RTE Integrator) Title : Quantitation For Method 525.2 *** Last Update : Mon Jun 03 15:34:22 2002 Response via : Initial Calibration DataAcq Meth : 052802

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-dlO 18.19 164 1899594 5.00 ug/L 0.00 9) Phenanthrene d-10 22.51 188 2868077 5.00 ug/L 0.00 19) Chrysene d-12 30.29 240 1857994 5.00 ug/L 0.00 25) p-Terphenyl d-14 27.39 244 2095758 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.11 134 538591 5.05 ug/L 0.00 Spiked Amount 5.000 Recovery = 101.00% 20) Triphenyl Phosphate 29.57 326 441636 5.59 ug/L 0.00 Spiked Amount 5.000 Recovery = 111.80% 21) Perylene D-12 34.30 264 705926 2.85 ug/L 0.00 Spiked Amount 5.000 Recovery a 57.00% 26) Acenaphthene d-10 (surr) 18.19 164 1899594 4.08 ug/L 0.00 Spiked Amount 5.000 Recovery = 81.60% 27) Phenanthrene d-10 (surr) 22.51 188 2868077 4.41 ug/L 0.00 Spiked Amount 5.000 Recovery = 88.20% 28) Chrysene d-12 (surr) 30.29 240 1857994 4.36 ug/L 0.00 Spiked Amount 5.000 Recovery = 87.20%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 0.00 165 0 N.D. 8) Molinate 0.00 126 0 N.D. 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 117 0 N.D. 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 0.00 129 0 N.D. d 23) Bis (2-Ethylhexyl) phthala 30.95 149 50484 0.81 ug/L 92 24) Benzo (a) pyrene 0.00 252 0 N.D.

(#) = qualifier out of range (m) = manual integration 11311RR.D 052802.M Mon Jun 03 15:50:01 2002 Page 1

NYC-WTC_000012617

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NYC-WTC_000012617Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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