GCMS pesticide analysis results, sample AE11573, May-June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Bath File : C:\MSDCHEM\1\DATA\052902\11311RR.D Vial: 16 : Acq On : 29 May 2002 2:39 pm Operator: Bohlk / Inst 213 Sample : SAMPLE 11311 RE-EXTD 5/23/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1\5973N\052802.M (RTE Integrator) Title : Quantitation For Method 525.2 *es Library : C: \DATABASE,\WILEY7N. L

Peak Number 5 Nonadecane (CAS) $$ n-Nonad... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 18.27 0.10 ug/L 141637 Acenaphthene-dl0 18.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Nonadecane (CAS) $$ n-Nonadecane 268 C19H40 000629-92-5 80 2 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 80 3 Heptadecane $$ n-Heptadecane $$__ 240 C17H36 000629-78-7 80 4 Docosane $$ n-Docosane $$ Normal 310 C22H46 000629-97-0 80 Abundance Scan 793 (18.269 mln): 11311RR.D (-) m/z 71.00 100.00%] 71

5000

55 11 99

, 127 _ALA ■n/z-> 0- AiLL 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 m/z 18.00 18.20 18.40 18.60 57.10 88.93%

Abundance #211487: Nonadecane (CAS) $$ n-Nonadecane 43 71 5000' -A । rri n r 18.00 18.20 18.40 18.60 m/z 85.10 73.85 x 99 . 27.11 1 J.. J. 127 154 183 0 111TTTTmnmmppmp 268 miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #245745: Heneicosane $$ n-Heneicosane 57

85 —Apr ALAAA 18.00 18.20 18.40 18.60 5000 m/z 99.10 34.82%

4'1 113. rf.., , . 54 . A. MA t -= it. . ■

n/z-> 0- 1544 J 141 . 169 197 225 253 Am* 296 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #174546: Heptadecane $$ n-Heptadecane $$ Normal-heptadecane 57 —AMA 18.00 18.20 18.40 18.60 m/z 55.10 19.48% 85 5000 41

! 1113 m/z—> 0 .15,1.4444,444.47+114192,-197.74 15 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 PMA rTO 18.00 18.20 18.40 18.60

311RR.D 052802.M Mon Jun 03 15:50:19 2002 Page 7

NYC-WTC_000012635