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GCMS pesticide analysis results, sample AE11911, May-June 2002

Machine-extracted title · confidence 100%

Laboratory report listing analytical results for pesticides and related compounds in a reference standard sample.

NYC-WTC_000012610–000012614

Folder label: “525 NOT OVR SAMPLE

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NYC 9/11 Public Portal Document yuaucLtatOI KepOrt (VL Kevlewed)

Data’File : C:\MSDCHEM\1\DATA\052902\11911.D Vial: 26 Acq On : 29 May 2002 9:33 pm Operator: Bohlk / Inst 213 Sample : SAMPLE 11911 5/23/02 Inst : Instrumen Mise Multipir: 1.00 MS Integration Params: rteint.p Quant Time: Jun 03 16:06:27 2002 Quant Results File: 052802.RES

Quant Method : C:\MSDCHEM\l\5973N\052802.M (RTE Integrator) 2" Title : Quantitation For Method 525.2 Last Update : Mon Jun 03 15:34:22 2002 Response via : Initial Calibration DataAcq Meth : 052802

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 18.19 164 2471459 5.00 ug/L 0.00 9) Phenanthrene d-10 22.51 188 3676436 5.00 ug/L 0.00 19) Chrysene d-12 30.29 240 2496838 5.00 ug/L 0.00 25) p-Terphenyl d-14 27.39 244 2790151 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3 -Dimethyl-2 -nitrobenzen 13.11 134 682029 4.92 ug/L 0.00 Spiked Amount 5.000 Recovery == 98.40% 20) Triphenyl Phosphate 29.57 326 605020 5.70 ug/L 0.00 Spiked Amount 5.000 Recovery = 114.00% 21) Perylene D-12 34.30 264 1650198 4.96 ug/L 0.00 Spiked Amount 5.000 Recovery s 99.20% 26) Acenaphthene d-10 (surr) 18.19 164 2471459 3.99 ug/L 0.00 Spiked Amount 5.000 Recovery = 79.80% 27) Phenanthrene d-10 (surr) 22.51 188 3676436 , 4.24 ug/L 0.00 Spiked Amount 5.000 Recovery = 84.80% 28) Chrysene d-12 (surr) 30.29 240 2496838 4.40 ug/L 0.00 Spiked Amount 5.000 Recovery = 88.00%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 0.00 165 0 N.D. . 8) Molinate 0.00 126 0 N.D. 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 117 0 N.D. 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 0.00 129 0 N.D. d 23) Bis (2-Ethylhexyl) phthala 30.95 149 280088 1.18 ug/L 97 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 11911.D 052802.M Mon Jun 03 16:07:19 2002 Page 1

NYC-WTC_000012611

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NYC-WTC_000012611Source: NYC Law Department, mirrored locally

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