GCMS analysis report, sample AE04451, April 2002

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Quantitation Report (QT Reviewed) % ■

Data File : C:\HPCHEM\l\DATA\MAR2102\4451.D Vial: 14 Acq On : 22 Mar 2002 12:06 am Operator: Sample : gc/ms scan 3/1 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 22 9:33 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 12.27 152 648740 20.00 ug/1 -0.08 10) Naphthalene-d8 15.90 136 2534796 20.00 ug/1 -0.09 17) Acenaphthene-diO 21.22 164 1347985 20.00 ug/1 -0.09 29) Phenanthrene-diO 25.66 188 2036705 20.00 ug/1 -0.10 38) Chrysene-dl2 33.72 240 1280861 20.00 ug/1 -0.12 44) Perylene-dl2 37.98 264 794187 20.00 ug/1 -0.14

System Monitoring Compounds 37) 2,4-DDD 30.73 235 83672 5.65 ug/mL 0.23 Spiked Amount 5.000 Recovery = 113.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2’-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.49 77 260 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Ac enapht hylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.52 165 295 N.D. 25) Diethylphthalate 22.69 149 107 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 2 8) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 4451.D GCMS0308.M Fri Mar 22 09:35:01 2002 Page 1

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