NYC-WTC_000012240
Calibration table for GC/MS analysis using Method 625/TCLP recorded on March 12 and 19, 2002.
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GCMS calibration data, Sample 2087, Mar 2002
Machine-extracted title · confidence 100%Calibration table for GC/MS analysis using Method 625/TCLP recorded on March 12 and 19, 2002.
NYC-WTC_000012258–000012263Folder label: “GCMS X 3-1-02 A 3-20-02 MANY RERNNS”
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NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed) 43 Data File e-\HPCHEM\1PATA\MAR1 102\2087.D Vial: 18 Acq On (12 Mar 2002/ 5:59 am Operator : Sample re-ext _ Inst . : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 19 12:00 2002 Quant Results File: GCMS0308.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.30 152 345383 20.00 ug/1 -0.05 10) Naphthalene-d8 15.94 136 1337876 20.00 ug/1 -0.06 17) Acenaphthene-diO 21.25 164 708265 20.00 ug/1 -0.07 29) Phenanthrene-diO 25.69 188 1093461 20.00 ug/1 -0.08 38) Chrysene-dl2 33.76 240 875237 20.00 ug/1 -0.09 44) Perylene-dl2 38.03 264 653761 20.00 ug/1 -0.09
System Monitoring Compounds 37) 2,4-DDD 30.77 235 70928 8.92 ug/mL > 0.27 Spiked Amount 5.000 Recovery =178.40%
Target Compounds alue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 ' N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 14.64 82 463 N.D. 13) bis(2-Chloroethoxy)methane 15.32 93 324 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.99 128 331 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachiorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 20.59 163 274 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.72 149 1003 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 2087.D GCMS0308.M Tue Mar 19 12:01:32 2002 Page 1
NYC-WTC_000012258
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