Calibration table for GC/MS analysis using Method 625/TCLP recorded on March 12 and 19, 2002.
NYC-WTC_000012200–000012206Folder label: “GCMS X 3-1-02 A 3-20-02 MANY RERNNS”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\MAR1102\1647.D Vial: 23 Acq On : 12 Mar 2002 12:53 pm Operator: Sample : re-ext fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 19 8:27 2002 Quant Results File: GCMS0308.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.30 152 355348 20.00 ug/1 -0.05 10) Naphthalene-d8 15.94 136 1384382 20.00 ug/1 -0.06 17) Acenaphthene-diO 21.24 164 734155 20.00 ug/1 -0.07 29) Phenanthrene-diO 25.70 188 1140452 20.00 ug/1 -0.07 38) Chrysene-dl2 33.76 240 927078 20.00 ug/1 -0.09 44) Perylene-dl2 38.03 264 700454 20.00 ug/1 -0.10
System Monitoring Compounds 37) 2,4-DDD 30.76 235 78997 9.53 ug/mB— .27 Spiked Amount 5.000 Recovery = 1190.60%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichiorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chioronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Ac enapht hylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.73 149 312 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 1647.D GCMS0308.M Tue Mar 19 08:28:47 2002 Page 1
NYC-WTC_000012200
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NYC-WTC_000012117
Laboratory report page for GC/MS analysis of sample AE01639 performed on March 25, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012258
Calibration table for GC/MS analysis using Method 625/TCLP recorded on March 12 and 19, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012170
Chromatogram and data from GC/MS analysis of sample AE01645 conducted on March 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012240
Calibration table for GC/MS analysis using Method 625/TCLP recorded on March 12 and 19, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012220
Calibration table for GC/MS analysis using Method 625/TCLP recorded on March 12 and 19, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012145
Chromatogram and data from GC/MS analysis of sample AE01640 conducted on March 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011942
Technical record of GCMS calibration data for TCLP analysis using sample vial 13 from March 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022850
Reviewed data file listing retention times and response factors for deuterated internal standards.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022812
Reviewed data file listing retention times and response factors for deuterated internal standards.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022909
GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022788
Reviewed data file listing retention times and response factors for deuterated internal standards.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022879
Reviewed data file listing retention times and response factors for deuterated internal standards.
1 shared topics · similarity 0.993
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NYC-WTC_000012083
Gas chromatography-mass spectrometry blank analysis for sample AE01639 completed March 21, 2002, with all organic compound detections below minimum detection limits.
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Calibration data for sample AE01639 verifying instrument performance for volatile organic compound analysis on March 21, 2002.
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