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GCMS calibration data, Sample 1647, Mar 2002

Machine-extracted title · confidence 100%

Calibration table for GC/MS analysis using Method 625/TCLP recorded on March 12 and 19, 2002.

NYC-WTC_000012200–000012206

Folder label: “GCMS X 3-1-02 A 3-20-02 MANY RERNNS

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR1102\1647.D Vial: 23 Acq On : 12 Mar 2002 12:53 pm Operator: Sample : re-ext fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 19 8:27 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.70 178 314 N.D. 34) Anthracene 25.70 178 315 N.D. 35) Di-n-butylphthalate 27.66 149 3304 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.76 228 2122 N.D. 42) Bis(2-ethylhexyl)phthalate 33.97 149 16265 0.44 ug/1 98 43) Chrysene 33.83 228 966 N.D. 45) Di-n-Octylphthalate 35.73 149 783 N.D. 46) Benzo(b)fluoranthene 36.83 252 280 N.D. 47) Benzo(k)fluoranthene 36.87 252 819 N.D. 4 8) Benzo(a)pyrene 38.04 252 2886 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo (g,h, i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 1647.D GCMS0308.M Tue Mar 19 08:28:51 2002 Page 2

NYC-WTC_000012201

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