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GCMS analysis results, Sample AE01645, Mar 2002

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Chromatogram and data from GC/MS analysis of sample AE01645 conducted on March 25, 2002.

NYC-WTC_000012170–000012175

Folder label: “GCMS X 3-1-02 A 3-20-02 MANY RERNNS

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR1102\1645.D Vial: 22 Acq On : 12 Mar 2002 11:54 am Operator : Sample : re-ext Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 19 8:26 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.30 152 336492 20.00 ug/1 -0.05 10) Naphthalene-d8 .15.94 136 1315326 20.00 ug/1 -0.06 17) Acenaphthene-diO 21.25 164 709796 20.00 ug/1 -0.07 2 9) Phenanthrene-dl0 25.69 188 1083116 20.00 ug/1 -0.08 38) Chrysene-dl2 33.76 240 886364 20.00 ug/1 -0.09 44) Perylene-dl2 38.03 264 655781 20.00 ug/1 -0.09

System Monitoring Compounds 37) 2,4-DDD 30.77 235 77154 9.80 ug/mL 0.27 Spiked Amount 5.000 Recovery = 196.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.99 128 302 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.72 149 1148 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 2 8) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 1645.D GCMS0308.M Tue Mar 19 08:27:03 2002 Page 1

NYC-WTC_000012170

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