NYC-WTC_000011415
Laboratory report documenting GCMS analysis of environmental sample AE03281 conducted on March 29, 2002.
Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Document / 16 pages
GCMS re-injection results, Sample 1639, Mar 2002
Machine-extracted title · confidence 100%Laboratory report for GC/MS re-injection of sample 1639 using Method 508 scan on March 20-21, 2002.
NYC-WTC_000012129–000012144Folder label: “GCMS X 3-1-02 A 3-20-02 MANY RERNNS”
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NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\1\DATA\031902\1640.D Vial: 25 Acq On : 20 Mar 2002 10:32 am Operator: McLean Sample : RE-INJ 3/1 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L
Peak Number 6 Octasiloxane , 1,1,3,3,5,5,7... Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
24.26 0.50 ug/L 207019 Phenanthrene-dl0 22.50
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Octasiloxane, 1,1,3,3,5,5,7,7,9, .. . 578 C16H5007Si8 019095-24-0 58 2 lH-Purin-6-amine, [(2-fluorophen... 243 C12H10FN5 074421-44-6 43 3 SILICONE POLYMER 458 C14H4205Si6 000000-00-0 40 4 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72O12Sil2 018919-94-3 37 Abundance Scan 2336 (24.264 min): 1640.D (-) m/z 73.10 100.00% 73
5000 147 221 281 24.00 24.20 24.40 24.60
m/z-> . 742. oV —TIHHr — 1’1"211130911010011131101301331110009033770T911"197 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 m/z 147.10 33.97%
Abundance #379834: Octasiloxane, 1.1,3,3.5,5,7,7.9,9.11,11,13.13,15,... 73
5000 207 T T ’I.T 24.00 24.20 24.40 24.60 281 m/z 281.00 25.35% 147 I 341 28,l J l 11 111385429 503 563 O' TTTfmmmmmememmmepmpmm miz—> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 Abundance #177443: 1H-Purin-6-amine, [(2-ftuorophenyl)methylJ- (CAS) 73
147 24.00 24.20 24.40 24.60 28, 221 5000 m/z 221.10 24.71% 355 281 429 503
miz-> 0- 0 lM 44ka— • * 4L 563607 653 703 TTpTT 50 100 150 200 250 300 350 400 450 500 550 600 650 700 Abundance 73 #392084: SILICONE POLYMER AmP— 24.00 24.20 24.40 24.60 m/z 355.10 11.50%
5000 147
221
281 . O-m —HH r*A .It hat. -r-rp-n-TT ' ‘ I ' ' ‘ ‘ I • m/z-> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 24.00 24.20 24.40 24.60
1640.D 5080302.M Thu Mar 21 06:31:34 2002 Page 8
NYC-WTC_000012141
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NYC-WTC_000012141Source: NYC Law Department, mirrored locally
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