NYC-WTC_000012240
Calibration table for GC/MS analysis using Method 625/TCLP recorded on March 12 and 19, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 6 pages
GCMS analysis results, Sample AE01639, Mar 2002
Machine-extracted title · confidence 100%Laboratory report page for GC/MS analysis of sample AE01639 performed on March 25, 2002, including surrogate recovery data.
NYC-WTC_000012117–000012122Folder label: “GCMS X 3-1-02 A 3-20-02 MANY RERNNS”
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NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\MAR1102\1639.D Vial: 20 Acq On : 12 Mar 2002 7:57 am Operator : Sample : re-ext fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 19 8:24 2002 Quant Results File: GCMS0308.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.30 152 339332 20.00 ug/1 -0.05 10) Naphthalene-d8 15.93 136 1331926 20.00 ug/1 -0.06 17) Acenaphthene-diO 21.24 164 698129 20.00 ug/1 -0.07 29) Phenanthrene-diO 25.69 188 1084604 20.00 ug/1 -0.07 38) Chrysene-dl2 33.75 240 879446 20.00 ug/1 -0.09 44) Perylene-dl2 38.02 264 652739 ' 20.00 ug/1 -0.10
System Monitoring Compounds 37) 2,4-DDD 30.77 235 75574 9.59 ug/mL 0.27 Spiked Amount .5.000 Recovery = 191.80%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.72 149 2555 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 1639.D GCMS0308.M Tue Mar 19 08:25:27 2002 Page 1
NYC-WTC_000012117
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Calibration table for GC/MS analysis using Method 625/TCLP recorded on March 12 and 19, 2002.
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Calibration table for GC/MS analysis using Method 625/TCLP recorded on March 12 and 19, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
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Calibration table for GC/MS analysis using Method 625/TCLP recorded on March 12 and 19, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012145
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