GCMS calibration table for TCLP analysis, March 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR2502\4386.D Vial: 13 Acq On : 25 Mar 2002 10:02 pm Operator: Sample : gc/ms scan 2/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 28 11:54 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Mar 26 14:13:06 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.26 152 452095 20.00 ug/1 -0.10 10) Naphthalene-d8 15.89 136 1734069 20.00 ug/1 -0.11 17) Acenaphthene-diO 21.20 164 938846 20.00 ug/1 -0.12 29) Phenanthrene-diO 25.63 188 1324316 20.00 ug/1 -0.13 38) Chrysene-dl2 33.69 240 700726 20.00 ug/1 -0.15 44) Perylene-dl2 37.93 264 422005 20.00 ug/1 -0.19

System Monitoring Compounds 5,3 37) 2,4-DDD 30.71 235 92845 8.56ug/mL 0.21 Spiked Amount 5.000 Recovery 171.20% /Dl% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.54 74 172 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichiorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.94 128 222 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chioronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.67 149 1526 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 2 7) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 4386.D GCMS0308.M Thu Mar 28 12:07:39 2002 Page 1

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