NYC-WTC_000011857
Laboratory report documenting GCMS analysis of environmental sample AE04388 conducted on April 3, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 12 pages
GCMS results for sample AE04412, April 2002
Machine-extracted title · confidence 100%Laboratory report documenting GCMS analysis of environmental sample AE04412 conducted on April 3, 2002.
NYC-WTC_000011893–000011904Folder label: “GCMS X 2/28/02 A 3/26/02”
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NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\MAR2502\4412.D Vial: 18 Acq On : 26 Mar 2002 2:58 am Operator: Sample : gc/ms scan 2/28 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
32.83 1.26 ug/1 127422 Chrysene-dl2 33.69
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3,6-Dioxa-2,4,5, 7-tetrasilaoctane, 294 C10H30O2Si4 004342-25-0 28 2 Trisiloxane, 1, 1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 16 3 1,1,1,3,5,5 ,7,7-Nonamethyl-3-(tri 384 C12H3604Si 5 038146-99-5 10 4 2,6-Dimethy -3;4-bis(trimethylsilyl 311 C15H29NO2Si2 000000-00-0 9 Abundance ...... Scan 3027 (32.831 min): 4412.D (-) /m/ Z " 73.00 100.00% 73 147 221
5000 281 355
3 49 429 32.60 32.80 33.00 33.20 ..... j.... . I a jl m/z~> 40 60 80 100 120 140160 180 200 220 240 260 280 300 320 340 360 380 400 42o " ' Abundance #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7- 147 221
73 5000 32.60 32.80 '33'00 33'20 191 117 m/z 221.05 69.43% miz-s I | J 279
40 60 80 100 120 140160 180 200 220 240 260 280 300 320 340 360 380 400 420 ' Abundance . ' : •. . • ' 1 - . . ppp 90009 “.. 73 147 32.60 32.80 33.00 33.20 5000 m/z 355.05 35.46% 281 / 45 369 117 207 249 miz-> 40 60 80'100120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420' ' Abundance 73 #52460:1,1.1,3,5.5,7,7,7-Nonamethyl-3-(trimethylsiloxy)tet _W 32.60 32.80 33.00 33.20 m/z 281.10 30.03% 281 5000 147
369 45 207 Cpmagmmmmmmam—mmanmmmpmammmgp m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 32.60 32.80 33.00 33.20
4412.D GCMS0308.M Thu Mar 28 12:35:32 2002 Page 3
NYC-WTC_000011902
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