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GCMS reference data for sample AE04038, April 2002

Machine-extracted title · confidence 100%

Reference analysis record for GCMS testing of sample AE04038 conducted on April 1, 2002, by analyst DLV.

NYC-WTC_000011719–000011727

Folder label: “GCMS X 2/25/02 A 3/23/02

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Scanned page image, NYC-WTC_000011724
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document 3 LSC Area Percent Report

’ Data File : C:\HPCHEM\l\DATA\MAR2202\4038.D Vial: 19 Acq On : 23 Mar 2002 1:47 pm Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.145 333 338 352 rBV 175989 417312 12.89% 2.584% 2 12.267 781 787 803 rVB 956501 2217054 68.48% 13.729% 3 15.902 1177 1183 1201 rBV 1459032 2965715 91.60% 18.365% 4 21.209 1755 1761 1777 rBV 1540006 3237608 100.00% 20.049% 5 25.661 2239 2246 2257 rBV2 1436177 3228019 99.70% 19.989%

6 30.729 2793 2798 2806 rBV 185943 386357 11.93% 2.393% 7 33.721 3113 3124 3139 rBV 955716 2242985 69.28% 13.890% 8 37.972 3579 3587 3604 rBV2 484761 1453549 44.90% 9.001%

Sum of corrected areas: 16148599

4038.D GCMS0308.M Wed Mar 27 09:59:52 2002

NYC-WTC_000011724

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NYC-WTC_000011724Source: NYC Law Department, mirrored locally

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