GCMS analysis results for sample AE03504, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

, Data File : C:\MSDCHEM\1\DATA\031202\3504.D Vial: 36 Acq On : 12 Mar 2002 5:46 pm Operator: McLean Sample : SAMPLE 3504 2/19/02 Inst s Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.56 3.05 ug/L 995001 1,4-Dichlorobenzene-d4 9.54

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tetr; ethyl- 88 C4H12Si 000075-76-3 9 2 2-(3-Methyl-: nitrobutyl)-1,3-di... 189 C8H15NO4 057620-56-1 9 3 3-Pentanol, j methyl- 102 C6H140 000077-74-7 9 43-(CYCLOHEx/ EN-YL) PROPANOL $$... 174 C8H1404 015745-87-6 9 Abundance 7 Scan 274 (5.561 min): 3504.D (-) m/z 73.10 100.00%| 73

5000

45 ■ i ■ • ■ ■ 1111111IITT 1114 ...................... . 5.20 5.40 5.60 5.80 87 193...................... m/z 45.10 14.49! 0- miz-> 0 20 40 60 80 100 120 140 160 180 Abundance #4814: Silane, tetramethyl- 73

5000 ■, ■. r. 1111'1111। A 5.20 5.40 5.60 5.80 m/z71.10 7.25 43 15 •a r29 1 55 2 ■ .A 0- TTT । PP-rr ■n*188 ‘ i ■ • • • i ■ ■ ■ ■ i 1 ■ • ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ miz-> 0 20 40 60 80 100 120 140 160 180 Abundance #98795:2-(3-Methyl-3-nitrobutyl)-1,3-dioxolane 73 ‘I T 1 • ■1 ■ 1 V 5.20 5.40 5.60 5.80 m/z55.10 4.69 5000

45 29 ।

/z-> 0- —1545— 86 99 114 0 20 40 60 •i th i r-| i i i i । i i 80 100 120 140 143 188 160 180* Abundance #9662: 3-Pentanol, 3-methyl- 73 AAARp 5.20 5.40 5.60 5.80 m/z69.10 4.50 55 5000 451 87 29

0—TPPIT —44 102 -Tmem m/z—> 0 20 40 60 80 100 120 140 160 180 5.20 5.40 5.60 5.80

3504.D 5080302.M Fri Mar 15 11:33:35 2002 Page 3

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