GCMS calibration data for Method 508, Mar 29 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

.•Data File : C:\MSDCHEM\l\DATA\032202\3437.D Vial: 43 Acq On : 22 Mar 2002 6:34 pm Operator: McLean Sample : 2/14/02 REINJ Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.56 1.73 ug/L 1180160 1,4-Dichlorobenzene-d4 9.55

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Silane, tetramethyl- 88 C4H12Si 000075-76-3 40 2 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 38 3 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 36 4 3-Pentanol, 2,4-dimethyl- 116 C7H160 000600-36-2 33 Abundance Scan 423 (5.565 min): 3437.D (-) m/z 73.20 100.00% 73

5000 43 ................ ,.........

5.20 5.40 5.60 5.80 6.00

•n/z-> 0- lalTin , 103 171 305 ‘T’TTIIUTTTIUUUTOTTTTTETETO ’TTTIOTOOOETTITTSIETT 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 m/z 43.10 36.79%

Abundance #4814: Silane, tetramethyl- 73

5000 FTTTntTtTtoar 5.20 5.40 5.60 5.80 6.00 m/z 45.20 13.94% 43 1,5 I, 0- TPWTTTITTTTT ■. ,'fi., ft j i.,.!..,. j, ।,.., (, H 11111111111 p rn-| 11111111111111 [ i n m/z-> 0 20 40 60 80 100120140160180 200 220 240 260280 300 Abundance #9663:3-Pentanol, 3-methyl- 73 1I99199TT 11 5.20 5.40 5.60 5.80 6.00 5000 m/z 41.20 12.80%

55

0- Is........ TrrTTpTTTp-rrrpTTTpT-rrj- miz-> 0 20 40 60 80 100120140160180200 220 240 260280 300 Abundance #9665:3-Pentanol, 3-methyl- " -AtM*? 1* .‘i 1. TTTTPem 73 5.20 5.40 5.60 5.80 6.00 m/z71.10 7.59%

5000 55

29 11 m/z-> 0 pl at m 0 20 40 60 80 100120140160180 200 220 240 260280 300 1 111 1111 5.20 5.40 5.60 5.80 6.00 Ympr

3437.D 5080302.M Mon Mar 25 11:20:15 2002 Page 3

NYC-WTC_000011573