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GCMS calibration results for sample AE03180, March 2002

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Laboratory report showing GC/MS calibration data and surrogate recovery for sample AE03180 on March 22, 2002.

NYC-WTC_000011162–000011164

Folder label: “GCMS X 2/12/02 A 3/19/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAR0102\3180.D Vial: 33 Acq On 2 Mar 2002 5:47 pm Operator: Sample gc/ms scan 2/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 5 14:19 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.29 168 494 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 3 2) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.77 178 3942 N.D. 34) Anthracene 25.91 178 2749 N.D. 35) Di-n-butylphthalate 27.68 149 9476 N.D. 36) Fluoranthene 29.43 202 4136 N.D. 3 9) Pyrene 30.10 202 4329 N.D. 40) Butylbenzylphthalate 32.21 149 2674 N.D. 41) Benzo(a)anthracene 33.85 228 4832 N.D. 42) Bis(2-ethylhexyl)phthalate 33.99 149 6019 N.D. 43) Chrysene 33.85 228 4735 N.D. 45) Di-n-Octylphthalate 35.73 149 2399 N.D. 46) Benzo(b)fluoranthene 36.85 252 2434 N.D. 47) Benzo(k)fluoranthene 36.92 252 3684 N.D. 4 8) Benzo(a)pyrene 37.85 252 1396 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 43.54 276 643 N.D.

(#) = qualifier out of range (m) = manual integration 3180.D GCMS0208.M Tue Mar 05 14:20:44 2002 Page 2

NYC-WTC_000011163

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NYC-WTC_000011163Source: NYC Law Department, mirrored locally

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