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GCMS blank analysis report for sample AE02713, March 4 2002

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Laboratory report documenting a blank run for gas chromatography-mass spectrometry analysis of sample AE02713.

NYC-WTC_000010843–000010861

Folder label: “GCMS X 2/5/02 A 2/28/02

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NYC 9/11 Public Portal Document LSC Area Percent Report .. Data File : C:\MSDCHEM\l\5973N\02FEB28\0205B.D Vial: 1 Acq On : 28 Feb 2002 10:30 am Operator: Sample : lab blank 2/5 Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\HP022102.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min . scan scan scan TY height area % max. total 1 3.611/ 17 21 29 rVB2 31954 65886 0.49% 0.092% 2 3.927/ 45 49 53 rBV 17339 30142 0.22% 0.042% 3 4.254 73 78 85 rBV2 9715 23401 0.17% 0.033% 4 4.638 107 112 115 rW 8140 13061 0.10% 0.018% 5 5.936/ 225 227 235 rBV 57022 143003 1.07% 0.200% 6 6.049 235 237 251 rVB 69633 204433 1.52% 0.286% 7 9.718 557 562 567 rBV 4002249 8158098 60.82% 11.400% 8 13.195 865 870 875 rBV 6189088 11934622 88.97% 16.678% 9 13.376/ 883 886 891 rVB 12445 30489 0.23% 0.043% 10 16.548 • 1163 1167 1171 rW 7271 16719 0.12% 0.023% 11 18.343 1319 1326 1331 rBV 6102694 12814924 95.53% 17.908% 12 19.980 1467 1471 1479 rBB 4667 14112 0.11% 0.020% 13 22.283 1671 1675 1681 rBV 40675 73946 0.55% 0.103% 14 22.644 1701 1707 1711 rBV2 5883434 13413918 100.00% 18.745% 15 22.768/ 1715 1718 1751 rVB 83998 443386 3.31% 0.620% 16 24.857 1897 1903 1913 rVB 11179 25761 0.19% 0.036% 17 27.724 I 2153 2157 2163 rBV 923181 1652469 12.32% 2.309% 18 29.677 ' 2327 2330 2335 rVB 6087 13284 0.10% 0.019% 19 30.490 2397 2402 2445 rBV2 5110192 12612696 94.03% 17.625% 20 34.418 2743 2750 2783 rBV 3568949 9875972 73.62% 13.801%

Sum of corrected areas: 71560322

0205B.D HP022102.M Fri Mar 01 10:06:44 2002 Page 1

NYC-WTC_000010846

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NYC-WTC_000010846Source: NYC Law Department, mirrored locally

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