GCMS calibration analysis results, DEP Labs, Feb 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

- ’ Data File : C:\MSDCHEM\l\5973N\02FEB21\0123B.D Vial: 1 Acq On : 21 Feb 2002 10:46 am Operator: Sample : lab blank 1/23 Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\HP022102.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.622 19 22 29 rBV2 34684 60583 0.42% 0.082% 2 3.927 45 49 55 rVB 18628 32742 0.23% 0.044% 3 4.649 109 113 117 rVB4 7271 16497 0.12% 0.022% 4 5.948 225 228 247 rVB 47434 144435 1.01% 0.195% 5 8.047 407 414 421 rVB4 2858 16411 0.11% 0.022%

6 9.718 557 562 567 rBV 4573512 8850081 61.84% 11.948% 7 9.899 573 578 587 rBV4 7009 28328 0.20% 0.038% 8 13.195 865 870 875 rBV 6761445 12953929 90.52% 17.488% 9 13.376 883 886 889 rVB2 11856 23631 0.17% 0.032% 10 14.539 979 989 995 rBV3 2231 14076 0.10% 0.019%

11 16.548 1163 1167 1171 rVB 11531 19485 0.14% 0.026% 12 18.343 1321 1326 1331 rBV 6644420 13865407 96.89% 18.718% 13 18.738 1357 1361 1369 rVB3 5518 15413 0.11% 0.021% 14 19.980 1467 1471 1481 rVB4 8556 27764 0.19% 0.037% 15 22.283 1671 1675 1685 rBV2 40677 86603 0.61% 0.117%

16 22.644 1701 1707 1711 rBV2 6179280 14311148 100.00% 19.320% 17 24.857 1899 1903 1909 rW2 7398 16304 0.11% 0.022% 18 27.724 2153 2157 2163 rBV 883359 1613255 11.27% 2.178% 19 30.490 2397 2402 2445 rBV2 5163528 12571668 87.85% 16.972% 20 34.407 2743 2749 2783 rBV 3334387 9406127 65.73% 12.698%

Sum of corrected areas: 74073887

0123B.D HP022102.M Mon Feb 25 10:54:36 2002 Page 1

NYC-WTC_000009921