GCMS results for vial 25, Feb 28 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\022702\02567.D Vial: 25 Acq ‘On : 28 Feb 2002 5:34 am Operator: McLean Sample : GC SCAN 2/4 B Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Mar 01 09:00:20 2002 Quant Results File: 5080202.RES

Quant Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Mon Feb 25 19:17:14 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.58 150 1722506 20.00 ug/L 0.00 10) Naphthalene-d8 13.05 136 4498852 20.00 ug/L 10 17) Acenaphthene-dlO 18.17 164 2504265 20.00 1 ' 0 29) Phenanthrene-diO 22.53 188 3866506 20 1 38) Chrysene-dl2 30.34 240 366431' 44) Perylene-dl2 34.22 264

System Monitoring Compounds 37) 2,4-ddd surr 27.47 Spiked Amount 5.000

Target Compounds 2) N-nitroso-dimethyl amine 3) bis(2-chloroethyl) ether 4) 1,3 - Dichlorobenze 5) 1,4 - Dichlorobenzene 0.00 0.00 0.00 0.00 14 146 o/{‘ 6) 1,2 - Dichlorobenzene 0.00 146 7) 2,2 ' - oxybis (l-Chloropr 0.00 45 8) N-Nitroso-di-n-propylamine 0.00 70 9) Hexachloroethane 0.00 117 11) Nitrobenzene 0.00 77 12) Isophorone 0.00 82 13) bis(2-Chloroethoxy) methan 0.00 93 14) 1,2,4-Trichlorobenzene 0.00 180 15) Naphthalene 0.00 128 16) Hexachlorobutadiene 0.00 225 18) Hexachlorocyclopentadiene 0.00 237 19) 2-chloronaphthalene 0.00 162 20) Dimethylphthalate 21) 2,6-Dinitrotoluene 22) Acenaphthylene 23) Acenaphthene 0.00 18.17 0.00 0.00 163 165 152 153 3137 u 24) 2,4-Dinitrotoluene 0.00 165 C 25) Diethylphthalate 0.00 149 0 26) 4-Chlorophenyl-phenyl ethe 0.00 204 0 27) Fluorene 0.00 166 0 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 30) N-Nitrosodiphenylamine 0.00 169 0 31) 4-Bromophenyl-phenyl ether 0.00 248 0 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 0.00 178 0 N.D. 3 4) Anthracene 0.00 178 0 N.D. 35) Di-n-butylphthalate 24.68 149 4146 0.02 ug/L 79 3 6) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo (a) antracene 30.34 228 9699 0.04 ug/L 57 42) Bis (2-ethylhexyl) phthala 30.94 149 11236 0.07 ug/L 93 43) Chrysene 30.34 228 9699 0.04 ug/L 55 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo (b) fluoranthene 0.00 252 0 N.D.

(#) = qualifier out of range (m) = manual integration 02567.D 5080202.M Fri Mar 01 09:00:48 2002 Page 1

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