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Document / 7 pages

GCMS calibration table results, February 27-March 19, 2002

Machine-extracted title · confidence 70%

Gas chromatography-mass spectrometry calibration analysis with retention times and response values for PAH standards and 2,4-DDD compound detection.

NYC-WTC_000010421–000010427

Folder label: “GCMS X 1/27/02 A 2/26/02 - 3/5/02 3/20/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\FEB25O2\1964 .D Vial: 36 Acq On : 27 Feb 2002 12:26 am Operator: Sample : gc/ms scan 1/29 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 19 10:49 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 0.00 178 0 N.D. 3 4) Anthracene 0.00 178 0 N.D. 35) Di-n-butylphthalate 27.68 149 1221 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.78 228 1313 N.D. 42) Bis(2-ethylhexyl)phthalate 33.99 149 904 N.D. 43) Chrysene 33.78 228 1313 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 38.05 252 1432 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 1964.D GCMS0208.M Tue Mar 19 10:50:07 2002 Page 2

NYC-WTC_000010422

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NYC-WTC_000010422Source: NYC Law Department, mirrored locally

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