GCMS analysis report for sample AE01507, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report . Data File : C:\MSDCHEM\1\5973N\02FEB21\01508.D Vial: 8 Acq On : 21 Feb 2002 9:01 pm Operator: Sample : 508 scan fb Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 9 Propanoic acid, 2-methyl-, . Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

9.89 0.07 ug/L 34398 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Propanoic acid, 2-methyl-, butyl... 144 C8H1602 000097-87-0 9 2 2-METHYL-3,3-D2-AZIRIDINE 59 C3H5D2N 030691-55-5 5 3 1-Butanamine 73 C4H11N 000109-73-9 5 4 3-cyano-3-methylhex-5-enamide $$... 152 C8H12N20 113661-30-6 4 Abundance Scan 577 (9.888 min): 01508.0 (-) m/z 59.10 100.00% 59

5000

41 | 73 86 152 9.60 N 9.80 10.00 10.20 0- ■ 11 • ■ ■ • i • ■ > • i • • ■ ■ 11 ■ ■ • i • mTT l * ’ 1 ‘ I ‘1 *71 ’ ‘ ‘ I H m/z *73.00 14.65% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #40313: Propanoic acid, 2-methyl-, butyl ester (CAS) $$ n-... 59

5000 71 .A 9.60 9.80 10.00 10.20 31 89 m/z 41.10 14.42% 44 129 144 0-mmmm H * i > * > • I' * ’ ' i ■ * ‘ * i ’ t11 • • i ’ ■ ’' i m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #500:2-METHYL-3,3-D2-AZIRiDINE 29 58

9.60 9.80 10.00 10.20 5000 m/z 44.00 12.26% 42 — oW 41aa1s*sg1*****as18at*[82098**g* niz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #1826:1-Butanamine • > I • - 33 9.60 9.80 10.00 10.20 m/z 42.10 11.02%

5000

miz—> 0 4 41 56 10 20 30 • ‘‘ i1 ■ 40 । 50 । 73 ।• i1"• i 60 70 80 ■ i ■■ ■11■1 ■ • i " “ i ■ ■' • i ■ ■ ■ ■ i■ "■ i" ■ ■ i 90 100 110 120 130 140 150 9.60 9.80 10.00 10.20

01508.D HP022102.M Mon Feb 25 10:54:57 2002 Page 11

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