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GCMS analysis results for sample AE01508, Mar 2002

Machine-extracted title · confidence 100%

Analytical results for sample AE01508 analyzed via GCMS on March 4, 2002, including surrogate recovery data.

NYC-WTC_000009966–000009985

Folder label: “GCMS X 1/23/02 A 2/21/02

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NYC 9/11 Public Portal Document LSC Area Percent Report File : C:\MSDCHEM\1\5973N\02FEB21\01507.D Vial: 4 in : 21 Feb 2002 1:24 pm Operator: ple : 508 scan Inst : Instrumen ■lisc : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\HP022102.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total 1 3.509 9 12 15 rVB2 16430 26337 0.16% 0.031% 2 3.633 21 23 25 rBV 32210 47945 0.30% 0.057% 3 3.938 47 50 53 rVB2 16603 27879 0.17% 0.033% 4 4.966 137 141 153 rVB6 7336 31606 0.20% 0.038% 5 5.948 225 228 245 rBV2 56060 200210 1.25% 0.238%

6 9.605 549 552 557 rBV3 8430 22138 0.14% 0.026% 7 9.718 557 562 567 rBV 5238394 9784480 61.07% 11.625% 8 9.887 575 577 593 rW2 10612 45609 0.28% 0.054% 9 13.195 865 870 875 rBV 7568613 14617949 91.25% 17.368% 10 13.376 883 886 897 rVB3 15212 46064 0.29% 0.055% 11 16.548 1163 1167 1171 rW 17997 29994 0.19% 0.036% 12 18.343 1321 1326 1331 rBV 7645261 15495937 96.73% 18.411% 13 19.980 1469 1471 1481 rVB3 14814 38478 0.24% 0.046% 14 21.334 1587 1591 1595 rVB 15415 22831 0.14% 0.027% 15 22.283 1671 1675 1681 rVB 45391 97097 0.61% 0.115% 16 22.644 1701 1707 1711 rBV2 7068654 16020474 100.00% 19.034% 17 24.857 1897 1903 1909 rBV 60712 141835 0.89% 0.169% 18 27.724 2153 2157 2163 rW 1099041 2007323 12.53% 2.385% 19 30.490 2397 2402 2435 rBV2 5641279 14281036 89.14% 16.968% 20 34.418 2743 2750 2773 rBV 4096704 11181415 69.79% 13.285%

Sum of corrected areas: 84166637

01507.D HP022102.M Mon Feb 25 10:54:49 2002 Page 1

NYC-WTC_000009970

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NYC-WTC_000009970Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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